1-Chloro-3-O-trityl-2-propanol

Base Information

• Chemical Name: 1-Chloro-3-O-trityl-2-propanol
• CAS No.: 69161-74-6
• Molecular Formula: C22H21ClO2
• Molecular Weight: 352.861
• Mol file: 69161-74-6.mol

Synonyms:1-Chloro-3-O-trityl-2-propanol;1-Chloro-3-(triphenylMethoxy)-2-propanol

Chemical Property of 1-Chloro-3-O-trityl-2-propanol

Chemical Property:

• PSA: 29.46000
• LogP: 4.59480
• Solubility.: Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

99% ^*data from raw suppliers

1-Chloro-3-O-trityl-2-propanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Oleoyl-3-chloropropanediol intermediate.

Technology Process of 1-Chloro-3-O-trityl-2-propanol

There total 2 articles about 1-Chloro-3-O-trityl-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

trityl chloride (76-83-5) + 3-monochloro-1,2-propanediol (96-24-2) → Rac-3-Chlor-1-O-trityl-1,2-propandiol (69161-74-6)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 25 ℃; for 24h;

DOI:10.1021/jo00031a053

Reference yield:

→ Rac-3-Chlor-1-O-trityl-1,2-propandiol (69161-74-6)

Guidance literature:

Tritylchlorid, 3-Chlor-1,2-propandiol;

DOI:10.1016/0009-3084(78)90020-8

Reference yield: 47.0%

vinyl acetate (108-05-4,9003-20-7) + Rac-3-Chlor-1-O-trityl-1,2-propandiol (69161-74-6) → Acetic acid (S)-1-chloromethyl-2-trityloxy-ethyl ester (138384-30-2)

Guidance literature:

In toluene; for 108h; Ambient temperature; lipase PS from Pseudomonas sp.;

DOI:10.1021/jo00031a053

upstream raw materials:

trityl chloride

3-monochloro-1,2-propanediol

Downstream raw materials:

3-Chlor-2-O-palmitoyl-1-O-trityl-propan-1,2-diol

Acetic acid (S)-1-chloromethyl-2-trityloxy-ethyl ester

(S)-1-Phenylsulfanyl-3-trityloxy-propan-2-ol

(R)-(+)-trityl glycidyl ether

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