2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione

Base Information

Chemical Name:2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione
CAS No.:950609-89-9
Molecular Formula:C₃₄H₄₀O₄Si₂
Molecular Weight:568.86
Hs Code.:
Mol file:950609-89-9.mol

Synonyms:2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione

Suppliers and Price of 2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione

Chemical Property:

Melting Point:>270 °C
Boiling Point:620.1±45.0 °C (760 mmHg)
PSA：52.60000
Density:1.111±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:9.53640

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione

There total 3 articles about 2,10-bis(tert-butyldiMethylsilyloxy)pentacene-6,13(5aH,13aH)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 950609-89-9
2,10-bis(tert-butyldimethylsiloxy)pentacene-6,13-dione

Guidance literature:

Reference yield:

: 229177-48-4
tert-butyl(3,4-dimethylphenoxy)dimethylsilane

: 950609-89-9
2,10-bis(tert-butyldimethylsiloxy)pentacene-6,13-dione

Guidance literature:: Multi-step reaction with 2 steps

1: NBS; AIBN / CCl₄ / 120 h / Heating

2: 1-butyl-3-methylimidazolium iodide / 2 h / 60 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane;
DOI:10.1021/jo0709807