5H-Pyrrolo[1,2-a]imidazole-6-carboxylicacid,6,7-dihydro-3-methyl-(9CI)

Base Information

• Chemical Name: 5H-Pyrrolo[1,2-a]imidazole-6-carboxylicacid,6,7-dihydro-3-methyl-(9CI)
• CAS No.: 408312-27-6
• Molecular Formula: C8H10N2O2
• Molecular Weight: 166.18
• Mol file: 408312-27-6.mol

Synonyms:5H-Pyrrolo[1,2-a]imidazole-6-carboxylicacid,6,7-dihydro-3-methyl-(9CI)

Chemical Property of 5H-Pyrrolo[1,2-a]imidazole-6-carboxylicacid,6,7-dihydro-3-methyl-(9CI)

Chemical Property:

Purity/Quality:

3-Methyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole-6-carboxylic acid ^*data from reagent suppliers

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Technology Process of 5H-Pyrrolo[1,2-a]imidazole-6-carboxylicacid,6,7-dihydro-3-methyl-(9CI)

There total 3 articles about 5H-Pyrrolo[1,2-a]imidazole-6-carboxylicacid,6,7-dihydro-3-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-3-methyl-5H-pyrrolo[1,2-a]imidazole-6-carboxylic acid (408312-40-3) → 3-methyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole-6-carboxylic acid (408312-27-6)

Guidance literature:

With sodium hydroxide; palladium on activated charcoal; Hydrogenation;

DOI:10.1002/hlca.19500330331

Reference yield:

3-methyl-2-oxo-2,3-dihydro-1H-pyrrolo[1,2-a]imidazole-6-carbonitrile (565453-80-7) → 3-methyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole-6-carboxylic acid (408312-27-6)

Guidance literature:

Multi-step reaction with 3 steps

1: POCl₃

2: aqueous HCl

3: palladium/charcoal; aq. NaOH solution / Hydrogenation

With hydrogenchloride; sodium hydroxide; palladium on activated charcoal; trichlorophosphate;

DOI:10.1002/hlca.19500330331

Reference yield:

2-chloro-3-methyl-5H-pyrrolo[1,2-a]imidazole-6-carbonitrile (857833-12-6) → 3-methyl-6,7-dihydro-5H-pyrrolo[1,2-a]imidazole-6-carboxylic acid (408312-27-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous HCl

2: palladium/charcoal; aq. NaOH solution / Hydrogenation

With hydrogenchloride; sodium hydroxide; palladium on activated charcoal;

DOI:10.1002/hlca.19500330331

upstream raw materials:

2-chloro-3-methyl-5H-pyrrolo[1,2-a]imidazole-6-carboxylic acid

3-methyl-2-oxo-2,3-dihydro-1H-pyrrolo[1,2-a]imidazole-6-carbonitrile

2-chloro-3-methyl-5H-pyrrolo[1,2-a]imidazole-6-carbonitrile

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