Technology Process of Tricyclo[4.1.1.02,5]octane
There total 6 articles about Tricyclo[4.1.1.02,5]octane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethanol;
DOI:10.1021/jo00362a022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 48 percent / KOH, H2O / ethane-1,2-diol / 1.5 h / 160 °C
2: CHCl3 / 173.5 - 200 °C / log k, ΔH, ΔS, olso photolysis
With
potassium hydroxide; water;
In
chloroform; ethylene glycol;
DOI:10.1021/jo00362a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 273 mg / H2, 5percent Pd/C / ethyl acetate / 30 h
2: 48 percent / KOH, H2O / ethane-1,2-diol / 1.5 h / 160 °C
3: CHCl3 / 173.5 - 200 °C / log k, ΔH, ΔS, olso photolysis
With
potassium hydroxide; palladium on activated charcoal; water; hydrogen;
In
chloroform; ethylene glycol; ethyl acetate;
DOI:10.1021/jo00362a022
