Methyl 2-(2,3-dichlorophenoxy)acetate

Base Information

• Chemical Name: Methyl 2-(2,3-dichlorophenoxy)acetate
• CAS No.: 1928-56-9
• Molecular Formula: C9H8Cl2O2
• Molecular Weight: 235.067
• European Community (EC) Number: 606-285-3
• DSSTox Substance ID: DTXSID401019395
• Mol file: 1928-56-9.mol

Synonyms:1928-56-9;Methyl 2-(2,3-dichlorophenoxy)acetate;2-(2,3-Dichlorophenoxy)-acetic acid methyl ester;Methyl-2-(2,3-Dichlorophenyl)Acetate;(2,3-dichlorophenoxy)-acetic acid methyl ester;SCHEMBL8816518;Methyl 2,3-dichlorophenoxyacetate;DTXSID401019395;AKOS005363262;J-505451

Chemical Property of Methyl 2-(2,3-dichlorophenoxy)acetate

Chemical Property:

• Vapor Pressure: 0.00112mmHg at 25°C
• Boiling Point: 300.5°C at 760 mmHg
• Flash Point: 125.4°C
• PSA: 35.53000
• Density: 1.352g/cm³
• LogP: 2.54520
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 233.9850495
• Heavy Atom Count: 14
• Complexity: 199

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(=O)COC1=C(C(=CC=C1)Cl)Cl

Technology Process of Methyl 2-(2,3-dichlorophenoxy)acetate

There total 2 articles about Methyl 2-(2,3-dichlorophenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dichlorophenol (576-24-9) + methyl chloroacetate (96-34-4) → (2,3-dichlorophenoxy)-acetic acid, methyl ester (1928-56-9)

Guidance literature:

2,3-dichlorophenol; With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 1h;

methyl chloroacetate; In N,N-dimethyl-formamide; at 50 ℃; for 12h;

DOI:10.1021/acs.jafc.9b03109

Reference yield:

→ (2,3-dichlorophenoxy)-acetic acid, methyl ester (1928-56-9)

Guidance literature:

/BRN= 43615/, ClCH2CO2CH3;

Reference yield:

(2,3-dichlorophenoxy)-acetic acid, methyl ester (1928-56-9) → 2,3-dichlorophenoxyacetic acid (2976-74-1)

Guidance literature:

With lithium hydroxide; In methanol; water; at 50 ℃; for 12h;

DOI:10.1021/acs.jafc.9b03109

upstream raw materials:

2,3-dichlorophenol

methyl chloroacetate

Downstream raw materials:

2,3-dichlorophenoxyacetic acid

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