n-(4-Amino-2-methoxyphenyl)-2-furamide

Base Information

• Chemical Name: n-(4-Amino-2-methoxyphenyl)-2-furamide
• CAS No.: 110506-35-9
• Molecular Formula: C12H12N2O3
• Molecular Weight: 232.24
• Hs Code.: 2932190090
• DSSTox Substance ID: DTXSID80353006
• Wikidata: Q82130450
• Mol file: 110506-35-9.mol

Synonyms:110506-35-9;n-(4-amino-2-methoxyphenyl)-2-furamide;N-(4-amino-2-methoxyphenyl)furan-2-carboxamide;Furan-2-carboxylic acid (4-amino-2-methoxy-phenyl)-amide;TimTec1_006413;Oprea1_168464;Oprea1_716612;2-Furancarboxamide, N-(4-amino-2-methoxyphenyl)-;DTXSID80353006;HMS1552D11;BBL000075;MFCD02258028;STK085706;AKOS000108398;VS-00429;BB 0245294;furan-2-carboxylic acid(4-amino-2-methoxy-phenyl)-amide;Furan-2-carboxylic acid (4-amino-2-methoxy-phenyl)-amide

Chemical Property of n-(4-Amino-2-methoxyphenyl)-2-furamide

Chemical Property:

• Melting Point: 113 °C(Solv: ethanol (64-17-5))
• Boiling Point: 325.6±37.0 °C(Predicted)
• PKA: 11.90±0.70(Predicted)
• PSA: 77.49000
• Density: 1.309±0.06 g/cm3(Predicted)
• LogP: 2.77690
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 232.08479225
• Heavy Atom Count: 17
• Complexity: 273

Purity/Quality:

97% ^*data from raw suppliers

N-(4-Amino-2-methoxyphenyl)furan-2-carboxamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=CC(=C1)N)NC(=O)C2=CC=CO2

Technology Process of n-(4-Amino-2-methoxyphenyl)-2-furamide

There total 6 articles about n-(4-Amino-2-methoxyphenyl)-2-furamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

Furan-2-carboxylic acid (2-methoxy-4-nitro-phenyl)-amide (110506-16-6) → furan-2-carboxylic acid-(4-amino-2-methoxy-anilide) (110506-35-9)

Guidance literature:

With hydrazine hydrate; nickel; In ethanol; for 2h; Heating;

Reference yield:

2-furancarbonyl chloride (527-69-5) → furan-2-carboxylic acid-(4-amino-2-methoxy-anilide) (110506-35-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / K₂CO₃ / acetone / Heating

2: 82 percent / 100percent N₂H₄*H₂O / Raney nickel / ethanol / 2 h / Heating

With potassium carbonate; hydrazine hydrate; nickel; In ethanol; acetone;

Reference yield:

2-methoxy-4-nitrophenylamine (97-52-9) → furan-2-carboxylic acid-(4-amino-2-methoxy-anilide) (110506-35-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / K₂CO₃ / acetone / Heating

2: 82 percent / 100percent N₂H₄*H₂O / Raney nickel / ethanol / 2 h / Heating

With potassium carbonate; hydrazine hydrate; nickel; In ethanol; acetone;

upstream raw materials:

Furan-2-carboxylic acid (2-methoxy-4-nitro-phenyl)-amide

2-furancarbonyl chloride

2-methoxy-4-nitrophenylamine

Downstream raw materials:

Furan-2-carboxylic acid (4-isothiocyanato-2-methoxy-phenyl)-amide

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