3-PHENYL-3'-TRIFLUOROMETHYLPROPIOPHENONE

Base Information

• Chemical Name: 3-PHENYL-3'-TRIFLUOROMETHYLPROPIOPHENONE
• CAS No.: 67082-01-3
• Molecular Formula: C16H13F3O
• Molecular Weight: 278.274
• Hs Code.: 2914700090
• Mol file: 67082-01-3.mol

Synonyms:3-PHENYL-3'-TRIFLUOROMETHYLPROPIOPHENONE

Chemical Property of 3-PHENYL-3'-TRIFLUOROMETHYLPROPIOPHENONE

Chemical Property:

• Vapor Pressure: 5.75E-05mmHg at 25°C
• Boiling Point: 346.5°C at 760 mmHg
• Flash Point: 187°C
• PSA: 17.07000
• Density: 1.201g/cm³
• LogP: 4.52090

Purity/Quality:

99% ^*data from raw suppliers

3-phenyl-3'-trifluoromethylpropiophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-PHENYL-3'-TRIFLUOROMETHYLPROPIOPHENONE

There total 3 articles about 3-PHENYL-3'-TRIFLUOROMETHYLPROPIOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(3-trifluoromethylphenyl)ethanol (454-91-1) + benzyl alcohol (100-51-6,185532-71-2) → 3-phenyl-1-(3-(trifluoromethyl)phenyl)propan-1-one (67082-01-3)

Guidance literature:

With C₁₆H₁₃MnN₅O₃⁽¹⁺⁾*Br^(1-); sodium hydroxide; In tert-Amyl alcohol; at 110 ℃; for 6h; Green chemistry;

DOI:10.1002/cssc.202000576

Reference yield: 82.0%

3'-(trifluoromethyl)acetophenone (349-76-8) + benzyl alcohol (100-51-6,185532-71-2) → 3-phenyl-1-(3-(trifluoromethyl)phenyl)propan-1-one (67082-01-3)

Guidance literature:

With dimanganese decacarbonyl; sodium hydroxide; In toluene; at 110 ℃; for 2h; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/acs.orglett.9b03030

Reference yield: 70.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3-(trifluoromethyl)benzoic acid (454-92-2) → 3-phenyl-1-(3-(trifluoromethyl)phenyl)propan-1-one (67082-01-3)

Guidance literature:

With 2,4,6-trimethyl-pyridine; methylene blue; triphenylphosphine; In N,N-dimethyl acetamide; at 20 ℃; Inert atmosphere; Irradiation;

upstream raw materials:

3'-(trifluoromethyl)acetophenone

benzyl alcohol

1-(3-trifluoromethylphenyl)ethanol

styrene

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