4-(6-CHLORO-2-PYRAZINYLCARBONYL)MORPHOLINE

Base Information

• Chemical Name: 4-(6-CHLORO-2-PYRAZINYLCARBONYL)MORPHOLINE
• CAS No.: 24079-32-1
• Molecular Formula: C9H10ClN3O2
• Molecular Weight: 227.65
• Hs Code.: 2934999090
• Mol file: 24079-32-1.mol

Synonyms:4-(6-CHLORO-2-PYRAZINYLCARBONYL)MORPHOLINE;4-[(6-chloro-2-pyrazinyl)carbonyl]morpholine(SALTDATA: FREE)

Chemical Property of 4-(6-CHLORO-2-PYRAZINYLCARBONYL)MORPHOLINE

Chemical Property:

• Vapor Pressure: 5.67E-07mmHg at 25°C
• Boiling Point: 411.2°C at 760 mmHg
• PKA: 0.00±0.10(Predicted)
• Flash Point: 202.5°C
• PSA: 55.32000
• Density: 1.388g/cm³
• LogP: 0.54030

Purity/Quality:

98% ^*data from raw suppliers

4-[(6-Chloro-2-pyrazinyl)carbonyl]morpholine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(6-CHLORO-2-PYRAZINYLCARBONYL)MORPHOLINE

There total 3 articles about 4-(6-CHLORO-2-PYRAZINYLCARBONYL)MORPHOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

morpholine (110-91-8,99108-56-2) + 6-chloropyrazine-2-carboxylic acid chloride (148673-71-6) → (6-chloropyrazin-2-yl)(morpholino)methanone (24079-32-1)

Guidance literature:

With triethylamine; In dichloromethane; for 2h; Inert atmosphere;

DOI:10.1039/c2ob25787d

Reference yield:

6-chloropyrazine-2-carboxylic acid (23688-89-3) → (6-chloropyrazin-2-yl)(morpholino)methanone (24079-32-1)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl chloride / dichloromethane

2: triethylamine / dichloromethane / 2 h

With oxalyl chloride; triethylamine; In dichloromethane;

DOI:10.1016/j.tetlet.2013.01.108

Reference yield:

→ (6-chloropyrazin-2-yl)(morpholino)methanone (24079-32-1)

Guidance literature:

2-(Morpholinocarbonyl)pyrazin-4-oxid,POCl3;

upstream raw materials:

morpholine

6-chloropyrazine-2-carboxylic acid chloride

6-chloropyrazine-2-carboxylic acid

Downstream raw materials:

C₂₁H₂₀N₃O₂P

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