2-Fluoro-4-Methoxy-1-(trifluoroMethyl)benzene

Base Information

• Chemical Name: 2-Fluoro-4-Methoxy-1-(trifluoroMethyl)benzene
• CAS No.: 1214344-33-8
• Molecular Formula: C₈H₆F₄O
• Molecular Weight: 194.129
• Hs Code.: 2909309090
• Mol file: 1214344-33-8.mol

Synonyms:2-Fluoro-4-Methoxy-1-(trifluoroMethyl)benzene;2-Fluoro-4-Methoxybenzotrifluoride

Chemical Property of 2-Fluoro-4-Methoxy-1-(trifluoroMethyl)benzene

Chemical Property:

• PSA: 9.23000
• LogP: 2.85310

Purity/Quality:

98%min ^*data from raw suppliers

2-Fluoro-4-methoxybenzotrifluoride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Fluoro-4-Methoxy-1-(trifluoroMethyl)benzene

There total 2 articles about 2-Fluoro-4-Methoxy-1-(trifluoroMethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

[nBu4N][Ag(2-fluoro-4-methoxylphenyl)(CF3)3] → [nBu4N][Ag(CF3)2] + 2-fluoro-4-methoxy-1-(trifluoromethyl)benzene (1214344-33-8)

Guidance literature:

In chloroform-d1; at 85 ℃; for 1h; Kinetics; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/acs.organomet.1c00195

Reference yield:

2-fluoro-4-methoxyphenyl pinalcolboronate (628692-21-7) + tetrabutylammomium bromide (1643-19-2) → [nBu4N][Ag(CF3)2] + 2-fluoro-4-methoxy-1-(trifluoromethyl)benzene (1214344-33-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: caesium carbonate / dimethyl sulfoxide / 1.5 h / 60 °C / Glovebox; Schlenk technique

1.2: 0.5 h / 20 °C / Glovebox; Schlenk technique

2.1: chloroform-d1 / 1 h / 85 °C / Inert atmosphere; Glovebox; Sealed tube

With caesium carbonate; In chloroform-d1; dimethyl sulfoxide;

DOI:10.1021/acs.organomet.1c00195

upstream raw materials:

2-fluoro-4-methoxyphenyl pinalcolboronate

tetrabutylammomium bromide

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