(5-CHLORO-6-METHYL-2-OXO-3-PHENETHYLAMINO-2H-PYRAZIN-1-YL)-ACETIC ACID

Base Information

Chemical Name:(5-CHLORO-6-METHYL-2-OXO-3-PHENETHYLAMINO-2H-PYRAZIN-1-YL)-ACETIC ACID
CAS No.:199296-28-1
Molecular Formula:C₁₅H₁₆ClN₃O₃
Molecular Weight:0
Hs Code.:

Synonyms:(5-CHLORO-6-METHYL-2-OXO-3-PHENETHYLAMINO-2H-PYRAZIN-1-YL)-ACETIC ACID;2-(5-chloro-6-methyl-2-oxo-3-(phenethylamino)pyrazin-1(2H)-yl)acetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5-CHLORO-6-METHYL-2-OXO-3-PHENETHYLAMINO-2H-PYRAZIN-1-YL)-ACETIC ACID

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Technology Process of (5-CHLORO-6-METHYL-2-OXO-3-PHENETHYLAMINO-2H-PYRAZIN-1-YL)-ACETIC ACID

There total 7 articles about (5-CHLORO-6-METHYL-2-OXO-3-PHENETHYLAMINO-2H-PYRAZIN-1-YL)-ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 64-04-0
phenethylamine

: 199296-19-0
3,5-dichloro-6-methyl-1-methylenecarboxypyrazinone

: 199296-28-1
3-(2-phenethylamino)-5-chloro-6-methyl-1-methylenecarboxypyrazinone

Guidance literature:: In 1,4-dioxane; at 65 ℃; for 16h;
DOI:10.1021/jm980368v

Reference yield:

: 199296-27-0
3-(2-phenethylamino)-5-chloro-6-methyl-1-benzyloxycarbonylmethylpyrazinone

: 199296-28-1
3-(2-phenethylamino)-5-chloro-6-methyl-1-methylenecarboxypyrazinone

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; for 15h; Yield given;
DOI:10.1021/jm980368v

Reference yield:

: Benzyl 2-[(1-cyanoethyl)amino]acetate hydrochloride

: 199296-28-1
3-(2-phenethylamino)-5-chloro-6-methyl-1-methylenecarboxypyrazinone

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dichloro-benzene / 100 °C

2: ethyl acetate / Heating

3: aq. LiOH / methanol; tetrahydrofuran

With lithium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; 1,2-dichloro-benzene;
DOI:10.1016/j.bmcl.2004.07.051