Methyl 1-[(4-Methoxyphenyl)Methyl]pyrrole-2-carboxylate

Base Information

• Chemical Name: Methyl 1-[(4-Methoxyphenyl)Methyl]pyrrole-2-carboxylate
• CAS No.: 900152-50-3
• Molecular Formula: C14H15NO3
• Molecular Weight: 245.2738
• Hs Code.: 2933990090
• Mol file: 900152-50-3.mol

Synonyms:Methyl 1-[(4-Methoxyphenyl)Methyl]pyrrole-2-carboxylate

Chemical Property of Methyl 1-[(4-Methoxyphenyl)Methyl]pyrrole-2-carboxylate

Chemical Property:

• PSA: 40.46000
• LogP: 2.33160

Purity/Quality:

95+% ^*data from raw suppliers

Methyl1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 1-[(4-Methoxyphenyl)Methyl]pyrrole-2-carboxylate

There total 1 articles about Methyl 1-[(4-Methoxyphenyl)Methyl]pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

methyl Pyrrole-2-carboxylate (1193-62-0) + p-methoxybenzyl chloride (824-94-2) → methyl 1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylate (900152-50-3)

Guidance literature:

With sodium hydroxide; In dichloromethane; water; at 18 ℃; for 16h;

DOI:10.1016/j.bmc.2006.02.018

Reference yield: 83.0%

methyl 1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylate (900152-50-3) → methyl 4,5-dibromo-1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylate (900152-51-4)

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 0 - 18 ℃; for 16h;

DOI:10.1016/j.bmc.2006.02.018

Reference yield: 80.0%

methyl 1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylate (900152-50-3) → 1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylic acid

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; ethanol; water; at 40 ℃;

DOI:10.1021/acs.jmedchem.7b00180

upstream raw materials:

methyl Pyrrole-2-carboxylate

p-methoxybenzyl chloride

Downstream raw materials:

methyl 4,5-dibromo-1-(4-methoxybenzyl)-1H-pyrrole-2-carboxylate

4-benzo[1,3]dioxol-5-yl-5-(3-hydroxy-4-methoxy-phenyl)-1-(4-methoxy-benzyl)-1H-pyrrole-2-carboxylic acid methyl ester

4-(3-hydroxy-4-methoxy-phenyl)-1-(4-methoxy-benzyl)-5-(3,4,5-trimethoxy-phenyl)-1H-pyrrole-2-carboxylic acid methyl ester

5-(3-hydroxy-4-methoxy-phenyl)-1-(4-methoxy-benzyl)-4-(3,4,5-trimethoxy-phenyl)-1H-pyrrole-2-carboxylic acid methyl ester

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