cis-3-(Boc-aMinoMethyl)cyclobutanol

Base Information

• Chemical Name: cis-3-(Boc-aMinoMethyl)cyclobutanol
• CAS No.: 917827-92-0
• Molecular Formula: C₁₀H₁₉NO₃
• Molecular Weight: 201.266
• Hs Code.: 2922500090
• Mol file: 917827-92-0.mol

Synonyms:cis-3-(Boc-aMinoMethyl)cyclobutanol;tert-Butyl ((cis-3-hydroxycyclobutyl)methyl)carbamate

Chemical Property of cis-3-(Boc-aMinoMethyl)cyclobutanol

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 319.899°C at 760 mmHg
• Flash Point: 147.27°C
• Density: 1.094g/cm³
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

cis-3-(Boc-aminomethyl)cyclobutanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-3-(Boc-aMinoMethyl)cyclobutanol

There total 10 articles about cis-3-(Boc-aMinoMethyl)cyclobutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

cis-3-(aminomethyl)cyclobutanol + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl (((cis)-3-hydroxycyclobutyl)methyl)carbamate (917827-92-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield:

3-(aminomethyl)cyclobutanol (167081-42-7) + di-tert-butyl dicarbonate (24424-99-5) → 3-(N-BOC-aminomethyl)-cyclobutanol (167081-41-6,917827-92-0)

Guidance literature:

In tetrahydrofuran; water;

Reference yield:

trans-3-(tert-butoxycarbonylaminomethyl)cyclobutyl 4-nitrobenzoate → tert-butyl ((trans-3-hydroxycyclobutyl)methyl)carbamate (917827-92-0)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃; for 12h;

upstream raw materials:

3-(aminomethyl)cyclobutanol

di-tert-butyl dicarbonate

N-benzyl-3-oxocyclobutanecarboxamide

3-oxocyclobutanecarboxylic acid

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