Dicyclopropa[cd,gh]pentalene, 1,1a-dichlorooctahydro-, (1-alpha-,1a-alpha-,1b-alpha-,2a-alpha-,2b-alpha-,2c-alpha-,2d-alpha-)- (9CI)

Base Information

• Chemical Name: Dicyclopropa[cd,gh]pentalene, 1,1a-dichlorooctahydro-, (1-alpha-,1a-alpha-,1b-alpha-,2a-alpha-,2b-alpha-,2c-alpha-,2d-alpha-)- (9CI)
• CAS No.: 103063-83-8
• Molecular Formula: C₈H₈Cl₂
• Molecular Weight: 175.058

Synonyms:Dicyclopropa[cd,gh]pentalene, 1,1a-dichlorooctahydro-, (1-alpha-,1a-alpha-,1b-alpha-,2a-alpha-,2b-alpha-,2c-alpha-,2d-alpha-)- (9CI)

Chemical Property of Dicyclopropa[cd,gh]pentalene, 1,1a-dichlorooctahydro-, (1-alpha-,1a-alpha-,1b-alpha-,2a-alpha-,2b-alpha-,2c-alpha-,2d-alpha-)- (9CI)

Chemical Property:

• Boiling Point: 241.8±13.0 °C(Predicted)
• Density: 1.54±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Technology Process of Dicyclopropa[cd,gh]pentalene, 1,1a-dichlorooctahydro-, (1-alpha-,1a-alpha-,1b-alpha-,2a-alpha-,2b-alpha-,2c-alpha-,2d-alpha-)- (9CI)

There total 8 articles about Dicyclopropa[cd,gh]pentalene, 1,1a-dichlorooctahydro-, (1-alpha-,1a-alpha-,1b-alpha-,2a-alpha-,2b-alpha-,2c-alpha-,2d-alpha-)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C8H9ClO → 2,3-exo-dichlorotetracyclo<3.3.0.02,8.04,6>octane (102968-84-3,103063-83-8) + 2,3-endo-dichlorotetracyclo<3.3.0.02,8.04,6>octane (102968-84-3,103063-83-8)

Guidance literature:

With triphenylphosphine; In tetrachloromethane; for 16h; Heating;

DOI:10.1002/hlca.19850680607

Reference yield:

C8H9ClO → 2,3-exo-dichlorotetracyclo<3.3.0.02,8.04,6>octane (102968-84-3,103063-83-8) + 2,3-endo-dichlorotetracyclo<3.3.0.02,8.04,6>octane (102968-84-3,103063-83-8)

Guidance literature:

With triphenylphosphine; In tetrachloromethane; for 16h; Heating;

DOI:10.1002/hlca.19850680607

Reference yield:

4,4-dichlorotetracyclo<3.3.0.02,8.03,6>octane → 2,3-exo-dichlorotetracyclo<3.3.0.02,8.04,6>octane (102968-84-3,103063-83-8) + 2,3-endo-dichlorotetracyclo<3.3.0.02,8.04,6>octane (102968-84-3,103063-83-8) + 4,6-endo-dichlorotricyclo<3.2.1.02,7>octane + 2,4-endo-dichlorobicyclo<3.2.1>octa-2,6-diene

Guidance literature:

In diethylene glycol dimethyl ether; at 190 ℃; for 24h; Yield given. Further byproducts given. Yields of byproduct given;

DOI:10.1002/hlca.19850680607

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