3-BROMOPHENYL CYCLOHEXYL KETONE

Base Information

• Chemical Name: 3-BROMOPHENYL CYCLOHEXYL KETONE
• CAS No.: 898769-06-7
• Molecular Formula: C13H15BrO
• Molecular Weight: 267.166
• Hs Code.: 2914700090
• Mol file: 898769-06-7.mol

Synonyms:3-BROMOPHENYL CYCLOHEXYL KETONE

Chemical Property of 3-BROMOPHENYL CYCLOHEXYL KETONE

Chemical Property:

• Vapor Pressure: 4.07E-05mmHg at 25°C
• Boiling Point: 351.6°C at 760 mmHg
• Flash Point: 64°C
• PSA: 17.07000
• Density: 1.338g/cm³
• LogP: 4.21210

Purity/Quality:

97% ^*data from raw suppliers

3-Bromophenylcyclohexylketone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BROMOPHENYL CYCLOHEXYL KETONE

There total 6 articles about 3-BROMOPHENYL CYCLOHEXYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.4%

(3-bromophenyl)(cyclohexyl)methanol → (3-bromophenyl)(cyclohexyl)methanone (898769-06-7)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 5h;

Reference yield: 42.0%

m-bromobenzoic aldehyde (3132-99-8) + cyclohexane (110-82-7,25012-93-5) → (3-bromophenyl)(cyclohexyl)methanone (898769-06-7)

Guidance literature:

With di-tert-butyl peroxide; at 180 ℃; for 1h; Microwave irradiation; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.joc.5b01824

Reference yield:

3-bromobenzoic acid isopropylamide (35306-75-3) → (3-bromophenyl)(cyclohexyl)methanone (898769-06-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 2-fluoropyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride; water / 20 °C

With hydrogenchloride; 2-fluoropyridine; water; In dichloromethane;

DOI:10.1002/cjoc.201900215

upstream raw materials:

m-bromobenzoic aldehyde

cyclohexane

1-bromocyclohexane

3-bromobenzoic acid isopropylamide

Downstream raw materials:

C₁₄H₁₈BrN₃S

C₁₅H₁₇BrN₂O₂

C₂₂H₂₄ClN₃O

C₁₆H₂₀BrN₃O

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