17β-Acetyl-estradiol 3-(Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester)

Base Information

• Chemical Name: 17β-Acetyl-estradiol 3-(Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester)
• CAS No.: 59495-70-4
• Molecular Formula: C₃₃H₄₂O₁₂
• Molecular Weight: 630.689
• Mol file: 59495-70-4.mol

Synonyms:17β-Acetyl-estradiol 3-(Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester);(17β)-17-Acetoxyestra-1,3,5(10)-trien-3-yl Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester;17-Acetyl-estradiol Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester

Chemical Property of 17β-Acetyl-estradiol 3-(Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester)

Chemical Property:

• PSA: 149.96000
• LogP: 3.54620
• Storage Temp.: Refrigerator
• Solubility.: Chloroform (Slightly), Methanol (Slightly, Heated)

Purity/Quality:

99% ^*data from raw suppliers

17β-Acetyl-estradiol3-(Tri-O-acetyl-β-D-glucuronicAcidMethylEster) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: A protected metabolite of Estradiol (E888000).

Technology Process of 17β-Acetyl-estradiol 3-(Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester)

There total 1 articles about 17β-Acetyl-estradiol 3-(Tri-O-acetyl-β-D-glucuronic Acid Methyl Ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

17-β-estradiol 17-acetate (1743-60-8) + (2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (7355-18-2) → methyl {(17β-acetoxy-1,3,5[10]-estratrien-3-yl)-2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate (59495-70-4)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃;

DOI:10.1080/07328309908544025

Reference yield: 84.0%

methyl {(17β-acetoxy-1,3,5[10]-estratrien-3-yl)-2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate (59495-70-4) → estradiol 3-O-glucuronide (15270-30-1,17263-23-9,21343-42-0,63307-54-0)

Guidance literature:

With sodium hydroxide; In methanol; at 20 ℃;

DOI:10.1080/07328309908544025

upstream raw materials:

17-β-estradiol 17-acetate

(2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl ester

Downstream raw materials:

estradiol 3-O-glucuronide

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