(12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine

Base Information

Chemical Name:(12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine
CAS No.:901773-53-3
Molecular Formula:C₁₄H₁₁N₃OS
Molecular Weight:269.327
Hs Code.:
DSSTox Substance ID:DTXSID00470845
Wikidata:Q82299025
Mol file:901773-53-3.mol

Synonyms:901773-53-3;(12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine;DTXSID00470845;2-Hydrazinyl-11H-naphtho[2',1':5,6]pyrano[4,3-d][1,3]thiazole

Suppliers and Price of (12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(12H-11-OXA-17-THIA-15-AZA-CYCLOPENTA[A]PHENANTHREN-16-YL)-HYDRAZINE 95.00%
1G
$ 1152.11

Total 0 raw suppliers

Chemical Property of (12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine

Chemical Property:

PSA：88.41000
LogP:3.91460
XLogP3:3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:269.06228316
Heavy Atom Count:19
Complexity:343

Purity/Quality:: (12H-11-OXA-17-THIA-15-AZA-CYCLOPENTA[A]PHENANTHREN-16-YL)-HYDRAZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2=C(C3=C(O1)C4=CC=CC=C4C=C3)N=C(S2)NN

Technology Process of (12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine

There total 2 articles about (12H-11-Oxa-17-thia-15-aza-cyclopenta[a]phenanthren-16-yl)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 93416-98-9
3-Bromo-4-oxo-2,3-dihydro-4H-naphtho<1,2-b>pyran

: 79-19-6
thiosemicarbazide

: 901773-53-3
(12H-11-oxa-17-thia-15-aza-cyclopenta[a]phenanthrene-16-yl)-hydrazine

Guidance literature:: In 1,4-dioxane; at 75 - 80 ℃; for 4h;
DOI:10.1016/j.ejmech.2006.01.018

Reference yield:

: 16563-51-2
benzo[h]chroman-4-one

: 901773-53-3
(12H-11-oxa-17-thia-15-aza-cyclopenta[a]phenanthrene-16-yl)-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / N-bromosuccinimide; benzoyl peroxide / CCl₄ / 4 h / Heating

2: 92 percent / dioxane / 4 h / 75 - 80 °C

With N-Bromosuccinimide; dibenzoyl peroxide; In 1,4-dioxane; tetrachloromethane;
DOI:10.1016/j.ejmech.2006.01.018