4-Phenylazulene

Base Information

Chemical Name:4-Phenylazulene
CAS No.:23781-83-1
Molecular Formula:C16H12
Molecular Weight:204.27
Hs Code.:2902909090
DSSTox Substance ID:DTXSID80547024
Nikkaji Number:J88.196A
Mol file:23781-83-1.mol

Synonyms:4-Phenylazulene;23781-83-1;4-Phenylazulen;DTXSID80547024

Suppliers and Price of 4-Phenylazulene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-Phenylazulene

Chemical Property:

PSA：0.00000
LogP:4.45840
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:204.093900383
Heavy Atom Count:16
Complexity:214

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=CC=C3C2=CC=C3

Technology Process of 4-Phenylazulene

There total 15 articles about 4-Phenylazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 50883-02-8
Diethyl 4-phenylazulene-1,3-dicarboxylate

: 23781-83-1
4-phenylazulene

Guidance literature:: With potassium hydroxide; In ethanol; for 2h; Heating;
DOI:10.1039/b003078n

Reference yield:

: 101269-60-7
4-phenyl-decahydro-azulene

: 23781-83-1
4-phenylazulene

Guidance literature:: With palladium on activated charcoal; at 350 - 360 ℃;
DOI:10.1021/ja01545a054

Reference yield:

: 106990-30-1
4-phenyl-octahydro-azulen-6-one

: 23781-83-1
4-phenylazulene

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄+H₂O; diethylene glycol / anschliessendes Erhitzen mit KOH

2: palladium/charcoal / 350 - 360 °C

With palladium on activated charcoal; hydrazine hydrate; diethylene glycol;
DOI:10.1021/ja01545a054