(2-Methyloxolan-2-yl)methanol

Base Information

• Chemical Name: (2-Methyloxolan-2-yl)methanol
• CAS No.: 81887-61-8
• Molecular Formula: C₆H₁₂O₂
• Molecular Weight: 116.16
• European Community (EC) Number: 866-395-4
• Nikkaji Number: J1.116.930I

Synonyms:(2-methyloxolan-2-yl)methanol;81887-61-8;tetrahydro-2-methyl-2-Furanmethanol;(2-methyltetrahydrofuran-2-yl)methanol;SCHEMBL2002220;AKOS018656815;SB73882;CS-0343241;FT-0749093;EN300-106293;Z1389059207

Chemical Property of (2-Methyloxolan-2-yl)methanol

Chemical Property:

• XLogP3: 0.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 116.083729621
• Heavy Atom Count: 8
• Complexity: 82.6

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CCCO1)CO

Technology Process of (2-Methyloxolan-2-yl)methanol

There total 1 articles about (2-Methyloxolan-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-allyl-2-methyl-oxirane (20924-80-5) → 2-methyl-1,4-pentanediol (6287-17-8) + 2-methyl-1,5-pentanediol (42856-62-2) + 4-methyl-1,4-pentanediol (1462-10-8) + (2-methyltetrahydrofuran-2-yl)methanol (81887-61-8)

Guidance literature:

With sodium hydroxide; borane; dihydrogen peroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 0 deg C, 2 h, 2.) THF, RT, 10 h;

Reference yield:

(2-methyltetrahydrofuran-2-yl)methanol (81887-61-8) → 2-hydroxy-N,N-dimethyl-3-(2-{[(5-methylfuran-2-yl)-(2-methyltetrahydrofuran-2-yl)methyl]amino}-3,4-dioxocyclobut-1-enylamino)benzamide + 2-hydroxy-N,N-dimethyl-3-(2-{[(5-methylfuran-2-yl)-(2-methyltetrahydrofuran-2-yl)methyl]amino}-3,4-dioxocyclobut-1-enylamino)benzamide

Guidance literature:

Multi-step reaction with 5 steps

1.1: pyridinium chlorochromate; silica gel / dichloromethane / 7 h / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / -70 - 20 °C

2.2: 3 h / -70 - 20 °C

3.1: diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 41 h / 0 - 20 °C

4.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 760.05 Torr

5.1: methanol / 3.5 h / 60 °C

With n-butyllithium; palladium 10% on activated carbon; diphenylphosphoranyl azide; hydrogen; silica gel; 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridinium chlorochromate; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; toluene;

upstream raw materials:

2-allyl-2-methyl-oxirane

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