(4R,4S)-BENZYL-4-DEOXY-4-C-NITROMETHYL-BETA-D-ARABINOPYRANOSIDE

Base Information

• Chemical Name: (4R,4S)-BENZYL-4-DEOXY-4-C-NITROMETHYL-BETA-D-ARABINOPYRANOSIDE
• CAS No.: 383173-66-8
• Molecular Formula: C₁₃H₁₇NO₆
• Molecular Weight: 283.281
• Mol file: 383173-66-8.mol

Synonyms:4-Benzyl-4-deoxy-4-C-nitromethyl-b-D-arabinopyranoside;PhenylMethyl 4-Deoxy-4-(nitroMethyl)-β-D-threo-pentopyranoside

Chemical Property of (4R,4S)-BENZYL-4-DEOXY-4-C-NITROMETHYL-BETA-D-ARABINOPYRANOSIDE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 488.755°C at 760 mmHg
• Flash Point: 249.39°C
• PSA: 104.74000
• Density: 1.361g/cm³
• LogP: 0.69740
• Solubility.: Ethyl Acetate, Methanol

Purity/Quality:

95% ^*data from raw suppliers

4-Benzyl-4-deoxy-4-C-nitromethyl-b-D-arabinopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4R,4S)-BENZYL-4-DEOXY-4-C-NITROMETHYL-BETA-D-ARABINOPYRANOSIDE

There total 2 articles about (4R,4S)-BENZYL-4-DEOXY-4-C-NITROMETHYL-BETA-D-ARABINOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (2R,3S,4S)-3,5-diacetoxy-2-benzyloxy-5-nitromethyl-tetrahydro-pyran-4-yl ester → Benzyl (4R)-4-deoxy-4-C-nitromethyl-β-D-arabino-pyranoside (383173-71-5,383173-66-8) + Benzyl (4S)-4-deoxy-4-C-nitromethyl-β-D-arabino-pyranoside (383173-66-8)

Guidance literature:

Acetic acid (2R,3S,4S)-3,5-diacetoxy-2-benzyloxy-5-nitromethyl-tetrahydro-pyran-4-yl ester; With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 0.916667h;

With methanol; sodium methylate; for 0.5h; Further stages.;

DOI:10.1002/1521-3765(20010903)7:17<3744::AID-CHEM3744>3.0.CO;2-3

Reference yield:

Acetic acid (2R,3S,4S)-3,5-diacetoxy-2-benzyloxy-5-nitromethyl-tetrahydro-pyran-4-yl ester → Benzyl (4R)-4-deoxy-4-C-nitromethyl-β-D-arabino-pyranoside (383173-71-5,383173-66-8) + Benzyl (4S)-4-deoxy-4-C-nitromethyl-β-D-arabino-pyranoside (383173-66-8)

Guidance literature:

Acetic acid (2R,3S,4S)-3,5-diacetoxy-2-benzyloxy-5-nitromethyl-tetrahydro-pyran-4-yl ester; With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 0.916667h;

With methanol; sodium methylate; for 0.5h; Further stages.;

DOI:10.1002/1521-3765(20010903)7:17<3744::AID-CHEM3744>3.0.CO;2-3

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