Methyl 2-((benzo[d]thiazol-2-ylsulfonyl)methyl)-3-bromo-6-methoxybenzoate

Base Information

• Chemical Name: Methyl 2-((benzo[d]thiazol-2-ylsulfonyl)methyl)-3-bromo-6-methoxybenzoate
• CAS No.: 1213268-13-3
• Molecular Formula: C₁₇H₁₄BrNO₅S₂
• Molecular Weight: 0
• Mol file: 1213268-13-3.mol

Synonyms:Methyl 2-((benzo[d]thiazol-2-ylsulfonyl)methyl)-3-bromo-6-methoxybenzoate

Chemical Property of Methyl 2-((benzo[d]thiazol-2-ylsulfonyl)methyl)-3-bromo-6-methoxybenzoate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

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MSDS Files:

SDS file from LookChem

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Technology Process of Methyl 2-((benzo[d]thiazol-2-ylsulfonyl)methyl)-3-bromo-6-methoxybenzoate

There total 1 articles about Methyl 2-((benzo[d]thiazol-2-ylsulfonyl)methyl)-3-bromo-6-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

methyl 2-{(benzo[d]thiazol-2-ylthio)methyl}-3-bromo-6-methoxybenzoate (1213268-10-0) → methyl 2-{(benzo[d]thiazol-2-ylsulfonyl)methyl}-3-bromo-6-methoxybenzoate (1213268-13-3)

Guidance literature:

With sodium tungstate (VI) dihydrate; dihydrogen peroxide; In methanol; at 0 - 20 ℃; for 6h;

DOI:10.1002/ejoc.200901012

Reference yield: 77.0%

methyl 2-{(benzo[d]thiazol-2-ylsulfonyl)methyl}-3-bromo-6-methoxybenzoate (1213268-13-3) + C28H30O6 → methyl 3-bromo-6-methoxy-2-{(E)-2-[(2R,4S,5R,6S)-3,4,5-tris-(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl]vinyl}benzoate

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200901012

Reference yield: 54.0%

methyl 2-{(benzo[d]thiazol-2-ylsulfonyl)methyl}-3-bromo-6-methoxybenzoate (1213268-13-3) + (3aR,4R,6aR)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxole-4-carbaldehyde (71165-16-7) → methyl 3-bromo-2-[(E)-2-{(3aS,4R,6aR)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl}vinyl]-6-methoxybenzoate (1213268-31-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200901012

upstream raw materials:

methyl 2-{(benzo[d]thiazol-2-ylthio)methyl}-3-bromo-6-methoxybenzoate

Downstream raw materials:

methyl 3-bromo-2-[(E)-2-{(3aS,4R,6aR)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl}vinyl]-6-methoxybenzoate

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