Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside

Base Information

Chemical Name:Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside
CAS No.:20197-44-8
Molecular Formula:C13H21NO7
Molecular Weight:303.31
Hs Code.:
Mol file:20197-44-8.mol

Synonyms:Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside

Suppliers and Price of Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside

Chemical Property:

Melting Point:153 - 154.5 °C (ethanol)
PSA：100.16000
LogP:0.13660

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside

There total 1 articles about Methyl 2-O,3-O-diacetyl-4-(acetylamino)-4,6-dideoxy-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (2R,3R,4S,5R,6S)-3-acetoxy-5-acetylamino-2-methoxy-6-methyl-tetrahydro-pyran-4-yl ester: 13042-65-4,13231-17-9,15856-47-0,17495-07-7,20197-44-8,24718-17-0,51255-07-3,51269-16-0,55570-19-9,58635-73-7
Acetic acid (2R,3R,4S,5R,6S)-3-acetoxy-5-acetylamino-2-methoxy-6-methyl-tetrahydro-pyran-4-yl ester

Guidance literature:: Pyranosid XIII a, Acetylierung;
DOI:10.7164/antibiotics.30.789

Reference yield:

: 20197-44-8
Methyl 4-acetamido-2,3-di-O-acetyl-4,6-dideoxy-α-D-mannopyranoside

: 141316-50-9
Methyl 4,6-dideoxy-4-<(1S)-(1,4/5,6)-4,5,6-trihydroxy-3-(hydroxymethyl)-2-cyclohexen-1-ylamino>-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: aq. hydrazine hydrate / 0.5 h / 70 °C

2: 2.) pyridine / 1.) 2-propanol, 50 deg C, 3 d, sealed tube

3: 81 percent / NaOMe / methanol / 1 h / Ambient temperature

With pyridine; sodium methylate; hydrazine hydrate; In methanol;
DOI:10.1016/0008-6215(92)84056-X