Technology Process of Tricyclo[3.3.1.13,7]decan-1-ethanesulfonaMide
There total 4 articles about Tricyclo[3.3.1.13,7]decan-1-ethanesulfonaMide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium permanganate;
In
water; acetone;
at 50 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ml300095a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sulfuryl dichloride; acetic anhydride / 1,2-dichloro-ethane / 0.5 h / -10 °C / Inert atmosphere
1.2: Inert atmosphere; Cooling with ice
2.1: potassium permanganate / water; acetone / 2 h / 50 °C / Inert atmosphere
With
potassium permanganate; sulfuryl dichloride; acetic anhydride;
In
water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ml300095a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
2.1: tetrahydrofuran / 60 °C / Inert atmosphere
3.1: sulfuryl dichloride; acetic anhydride / 1,2-dichloro-ethane / 0.5 h / -10 °C / Inert atmosphere
3.2: Inert atmosphere; Cooling with ice
4.1: potassium permanganate / water; acetone / 2 h / 50 °C / Inert atmosphere
With
1H-imidazole; potassium permanganate; sulfuryl dichloride; iodine; acetic anhydride; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ml300095a
