6-BroMo-3-Methyl-2-pyridinaMine

Base Information

• Chemical Name: 6-BroMo-3-Methyl-2-pyridinaMine
• CAS No.: 89466-16-0
• Molecular Formula: C6H7BrN2
• Molecular Weight: 187.039
• Hs Code.: 2933399090
• Mol file: 89466-16-0.mol

Synonyms:6-BroMo-3-Methyl-2-pyridinaMine;6-BroMo-3-Methylpyridin-2-aMine;2-Amino-6-bromo-3-methylpyridine

Chemical Property of 6-BroMo-3-Methyl-2-pyridinaMine

Chemical Property:

• Boiling Point: 289.5±35.0 °C(Predicted)
• PKA: 3.08±0.50(Predicted)
• PSA: 38.91000
• Density: 1.593±0.06 g/cm3(Predicted)
• LogP: 2.31590
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

99%, ^*data from raw suppliers

6-Bromo-3-methylpyridin-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 6-Bromo-3-methylpyridin-2-amine can be used as factor D inhibitors for treatment of immune and inflammatory disorders.

Technology Process of 6-BroMo-3-Methyl-2-pyridinaMine

There total 4 articles about 6-BroMo-3-Methyl-2-pyridinaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromo-N-tert-butyl-3-methylpyridin-2-amine → 6-bromo-3-methylpyridin-2-amine (89466-16-0)

Guidance literature:

With trifluoroacetic acid; at 65 ℃; for 6h; Large scale;

Reference yield:

2-Bromo-5-methylpyridine (3510-66-5) → 6-bromo-3-methylpyridin-2-amine (89466-16-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 25 °C / Large scale

2.1: dichloromethane / 0.17 h / -25 °C / Large scale

2.2: 2 h / -25 °C / Large scale

3.1: trifluoroacetic acid / 6 h / 65 °C / Large scale

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane;

Reference yield:

2-Bromo-5-methylpyridine N-oxide (19230-58-1) → 6-bromo-3-methylpyridin-2-amine (89466-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: dichloromethane / 0.17 h / -25 °C / Large scale

1.2: 2 h / -25 °C / Large scale

2.1: trifluoroacetic acid / 6 h / 65 °C / Large scale

With trifluoroacetic acid; In dichloromethane;

upstream raw materials:

2-Bromo-5-methylpyridine

2-Bromo-5-methylpyridine N-oxide

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