Technology Process of 3-Cyano-2-iodobenzoic acid
There total 6 articles about 3-Cyano-2-iodobenzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) SOCl2
2: aq. NaOH / methanol / 1 h / Heating
3: SOCl2 / 1 h / Heating
4: NH4OH / CH2Cl2
5: 59 percent / POCl3 / 1 h / 100 °C
6: 100 percent / aq. NaOH / methanol / Heating
With
ammonium hydroxide; sodium hydroxide; thionyl chloride; trichlorophosphate;
In
methanol; dichloromethane;
DOI:10.1021/jm00387a013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. NaOH / methanol / 1 h / Heating
2: SOCl2 / 1 h / Heating
3: NH4OH / CH2Cl2
4: 59 percent / POCl3 / 1 h / 100 °C
5: 100 percent / aq. NaOH / methanol / Heating
With
ammonium hydroxide; sodium hydroxide; thionyl chloride; trichlorophosphate;
In
methanol; dichloromethane;
DOI:10.1021/jm00387a013
