NSC 21394-d5

Base Information

• Chemical Name: NSC 21394-d5
• CAS No.: 697806-98-7
• Molecular Formula: C₄H₆N₂
• Molecular Weight: 87.0653
• Mol file: 697806-98-7.mol

Synonyms:1H-2-MethyliMidazole-d5;2-Methyl-1H-iMidazole-d5;2-MethyliMidazole-d5;2MZ-d5;2MZ-H-d5;2MZ-PW-d5;Actiron 2MI-d5;Curezol 2MZ-d5

Chemical Property of NSC 21394-d5

Chemical Property:

• PSA: 28.68000
• LogP: 0.71810

Purity/Quality:

97% ^*data from raw suppliers

2-Methylimidazole-d5(Major) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (2-Methylimidazole-d5) Labelled 2-Methylimidazole (M312985). 2-Methylimidazole is a monomethylated imidazole that can be used as a building block in the preparation of a wide range of biologically active compounds. 2-Methylimidazole as well as other imidazoles can be use as catalyst for refolding of enhanced coloured fluorescent protein. 2-Methylimidazole has been identified as a byproduct of fermentation and is detected in foods and mainstream and side-stream tobacco smoke.

Technology Process of NSC 21394-d5

There total 1 articles about NSC 21394-d5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-methylimidazole (693-98-1) → 2-methylimidazole-d5 (697806-98-7)

Guidance literature:

With hydrogen; water-d2; palladium 10% on activated carbon; at 160 ℃; for 24h; Product distribution / selectivity;

Reference yield:

dioxygen-(16)O (1173018-52-4) + [(meso-tetra(α,α,α,α-ortho-pivalamidophenyl)porphyrin)cobalt(II)] (87680-78-2,87680-77-1,53675-31-3,87680-79-3,87680-76-0) + 2-methylimidazole-d5 (697806-98-7) → Co(((CH3)3CCONHC6H4)4C20H8N4)(C(2)H3C3(2)H2N2H)(16)O2

Guidance literature:

In dichloromethane; degassed solvent vac. transferred to solid mixt. of metalloporphyrin and the nitrogeneous base, oxygen introduced momentarily (less than 2 s) to frozen sample (liq. N2); not isolated; detected by Raman spectroscopy;

DOI:10.1021/ja00337a017

upstream raw materials:

2-methylimidazole

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