(S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)acetic acid

Base Information

• Chemical Name: (S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)acetic acid
• CAS No.: 1228547-87-2
• Molecular Formula: C₁₃H₁₆BrNO₄
• Molecular Weight: 330.178
• Mol file: 1228547-87-2.mol

Synonyms:(S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)acetic acid

Chemical Property of (S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)acetic acid

Chemical Property:

• Boiling Point: 456.3±40.0 °C(Predicted)
• PKA: 3.26±0.10(Predicted)
• PSA: 75.63000
• Density: 1.443±0.06 g/cm3(Predicted)
• LogP: 3.49040
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

95+% ^*data from raw suppliers

(S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)aceticacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of (S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)acetic acid

There total 1 articles about (S)-2-(2-Bromophenyl)-2-((tert-butoxycarbonyl)amino)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (S)-α-amino-α-(2-bromophenyl)acetic acid hydrochloride (1313219-33-8) → C13H16BrNO4 (1228547-87-2)

Guidance literature:

With sodium hydrogencarbonate; In water; tert-butyl alcohol; for 5h;

DOI:10.1016/j.tet.2009.04.098

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + C13H16BrNO4 (1228547-87-2) → methyl N-Boc-(S)-2-(2-bromophenyl)glycinate (1176305-56-8)

Guidance literature:

In ethyl acetate; optical yield given as %ee;

DOI:10.1016/j.tet.2009.04.098

upstream raw materials:

di-tert-butyl dicarbonate

(S)-α-amino-α-(2-bromophenyl)acetic acid hydrochloride

Downstream raw materials:

methyl N-Boc-(S)-2-(2-bromophenyl)glycinate

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