ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME

Base Information

• Chemical Name: ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME
• CAS No.: 70427-91-7
• Molecular Formula: C₁₃H₂₄O₁₁
• Molecular Weight: 356.327
• Hs Code.: 29389090
• Mol file: 70427-91-7.mol

Synonyms:METHYL 4-O-ALPHA-D-MANNOPYRANOSYL-ALPHA-D-MANNOPYRANOSIDE;ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME;methyl 4-O-A-D-mannopyranosyl-A-D-*mannopyranosid;METHYL 4-O-A-D-MANNOPYRANOSYL-A-D-*MANNO PYRANOSIDE;methyl 4-o-α-d-mannopyranosyl-α-d-mannopyranoside;α-d-man-[1→4]-α-d-man-1→ome

Chemical Property of ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME

Chemical Property:

• PSA: 178.53000
• LogP: -4.74310
• Storage Temp.: −20°C

Purity/Quality:

99% ^*data from raw suppliers

Methyl4-O-(α-D-mannopyranosyl)-α-D-mannopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME

There total 54 articles about ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

methyl 2,3,6-tri-O-benzyl-4-O-{3,4,6-tri-O-benzyl-2-O-[3'-(2''-benzyloxyphenyl)-3',3'-dimethylpropanoyl]-β-D-glucopyranosyl}-(1->4)-α-D-glucopyranoside (935554-58-8) → methyl 4-O-β-D-glucopyranosyl-(1->4)-α-D-glucopyranoside (744-05-8,4198-49-6,7216-69-5,7216-73-1,21973-65-9,35438-39-2,58462-71-8,66101-74-4,66101-75-5,67145-39-5,67145-40-8,70399-66-5,70427-91-7,70428-28-3,80446-84-0,81131-44-4,84129-57-7,92282-08-1,93221-82-0,114580-08-4,114817-99-1,117064-58-1,117064-59-2,118493-11-1,118493-12-2,118493-13-3,127253-90-1,127641-09-2,130192-72-2,136890-91-0,145680-83-7,146683-50-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; at 20 ℃; for 5h; under 2280.15 Torr;

DOI:10.1021/ol070449y

Reference yield: 93.0%

3,6,2',3',4',6'-hexa-O-acetyl-α-cellobioside (77068-23-6) → methyl 4-O-β-D-glucopyranosyl-(1->4)-α-D-glucopyranoside (744-05-8,4198-49-6,7216-69-5,7216-73-1,21973-65-9,35438-39-2,58462-71-8,66101-74-4,66101-75-5,67145-39-5,67145-40-8,70399-66-5,70427-91-7,70428-28-3,80446-84-0,81131-44-4,84129-57-7,92282-08-1,93221-82-0,114580-08-4,114817-99-1,117064-58-1,117064-59-2,118493-11-1,118493-12-2,118493-13-3,127253-90-1,127641-09-2,130192-72-2,136890-91-0,145680-83-7,146683-50-3)

Guidance literature:

With sodium methylate; In methanol; for 2h; Ambient temperature;

DOI:10.1016/S0008-6215(00)85548-2

Reference yield: 92.0%

methyl (β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside (88559-79-9) → methyl 4-O-β-D-glucopyranosyl-(1->4)-α-D-glucopyranoside (744-05-8,4198-49-6,7216-69-5,7216-73-1,21973-65-9,35438-39-2,58462-71-8,66101-74-4,66101-75-5,67145-39-5,67145-40-8,70399-66-5,70427-91-7,70428-28-3,80446-84-0,81131-44-4,84129-57-7,92282-08-1,93221-82-0,114580-08-4,114817-99-1,117064-58-1,117064-59-2,118493-11-1,118493-12-2,118493-13-3,127253-90-1,127641-09-2,130192-72-2,136890-91-0,145680-83-7,146683-50-3)

Guidance literature:

palladium on activated charcoal; In acetic acid; for 24h; under 760 Torr; Ambient temperature;

DOI:10.1016/0008-6215(83)84014-2

upstream raw materials:

barium methoxide

methyl-[O²,O³,O⁶-triacetyl-O⁴-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-mannopyranoside]

2,3,4,6-tetra-O-benzoylglucosyl bromide

methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Downstream raw materials:

methyl 4-O-(2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl)-2,3-di-O-acetyl-6-O-benzyl-α-D-glucopyranoside

methyl 4-O-(3-O-benzyl-4,6-O-benzylidene-α-D-glucopyranosyl)-6-O-benzyl-α-D-glucopyranoside

methyl 2,3,6,2',3'-penta-O-acetyl-4',6'-O-benzylidene-α-maltoside

formic acid

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