4-Methyl-3-furancarboxylic acid

Base Information

• Chemical Name: 4-Methyl-3-furancarboxylic acid
• CAS No.: 101870-15-9
• Molecular Formula: C6H6O3
• Molecular Weight: 126.112
• Mol file: 101870-15-9.mol

Synonyms:4-Methyl-3-furancarboxylic acid

Chemical Property of 4-Methyl-3-furancarboxylic acid

Chemical Property:

• PSA: 50.44000
• LogP: 1.28620

Purity/Quality:

99% ^*data from raw suppliers

4-Methyl-3-furancarboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methyl-3-furancarboxylic acid

There total 15 articles about 4-Methyl-3-furancarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-methyl-furan-3-carboxylic acid methyl ester (57279-03-5) → 4-methyl-3-furancarboxylic acid (101870-15-9)

Guidance literature:

With potassium hydroxide; at 20 ℃; for 18h;

Reference yield:

2-(tert-Butyl-dimethyl-silanyl)-4-methyl-furan-3-carboxylic acid (137304-11-1) → 4-methyl-3-furancarboxylic acid (101870-15-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1021/jo971098b

Reference yield:

2-(tert-Butyl-dimethyl-silanyl)-furan-3-carboxylic acid (133620-36-7) → 4-methyl-3-furancarboxylic acid (101870-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) HMPA / 1.) DME, -20 deg C, 1 h, 2.) THF, 0 deg C, 6 h

2: n-Bu₄NF / tetrahydrofuran / 1 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran;

DOI:10.1021/jo971098b

upstream raw materials:

4-methyl-furan-2,3-dicarboxylic acid

4-methyl-furan-3-carboxylic acid methyl ester

2-(tert-Butyl-dimethyl-silanyl)-4-methyl-furan-3-carboxylic acid

2-(tert-Butyl-dimethyl-silanyl)-furan-3-carboxylic acid

Downstream raw materials:

4-methyl-furan-3-carboxylic acid methyl ester

tautomycin

methyl 3-(4-methylfuran-3-yl)-3-oxopropanoate

(R)-3-(Diethyl-isopropyl-silanyloxy)-3-(4-methyl-furan-3-yl)-propionic acid benzyl ester

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