Technology Process of Oxiranecarboxylic acid, 3-(chlorocarbonyl)-, ethyl ester (9CI)
There total 6 articles about Oxiranecarboxylic acid, 3-(chlorocarbonyl)-, ethyl ester (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1002/poc.3683
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen bromide / 6.25 h / 0 - 20 °C
2: hydrogen bromide / acetic acid; ethanol / 10 h / Reflux
3: potassium carbonate / acetone / 0 - 20 °C
4: potassium hydroxide / ethanol / 0 - 20 °C
5: oxalyl dichloride / dichloromethane / 0 - 20 °C
With
oxalyl dichloride; hydrogen bromide; potassium carbonate; potassium hydroxide;
In
ethanol; dichloromethane; acetic acid; acetone;
DOI:10.1002/poc.3683
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen bromide / acetic acid; ethanol / 10 h / Reflux
2: potassium carbonate / acetone / 0 - 20 °C
3: potassium hydroxide / ethanol / 0 - 20 °C
4: oxalyl dichloride / dichloromethane / 0 - 20 °C
With
oxalyl dichloride; hydrogen bromide; potassium carbonate; potassium hydroxide;
In
ethanol; dichloromethane; acetic acid; acetone;
DOI:10.1002/poc.3683