4-CHLORO-5-METHOXY-1-INDANONE

Base Information

• Chemical Name: 4-CHLORO-5-METHOXY-1-INDANONE
• CAS No.: 944109-65-3
• Molecular Formula: C₁₀H₉ClO₂
• Molecular Weight: 196.633
• Hs Code.: 2914700090
• Mol file: 944109-65-3.mol

Synonyms:4-CHLORO-5-METHOXY-1-INDANONE;4-Chloro-5-Methoxy-2,3-dihydro-1H-inden-1-one;4-Chloro-5-methoxy-1-indanone 97%;4-Chloro-5-methoxy-indan-1-one

Chemical Property of 4-CHLORO-5-METHOXY-1-INDANONE

Chemical Property:

• Melting Point: 124-128 °C
• PSA: 26.30000
• LogP: 2.47750
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

4-chloro-5-methoxy-1-indanone ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-5-METHOXY-1-INDANONE

There total 2 articles about 4-CHLORO-5-METHOXY-1-INDANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

5-methoxy-1-indanone (5111-70-6) → 4-chloro-5-methoxy-2,3-dihydro-1H-inden-1-one (944109-65-3)

Guidance literature:

With sodium hypochlorite; acetic acid; In water; at 0 - 17 ℃; for 3.33333h;

Reference yield: 74.0%

5-methoxy-1-indanone (5111-70-6) → 4-chloro-5-methoxy-2,3-dihydro-1H-inden-1-one (944109-65-3) + 6-chloro-5-methoxy-2,3-dihydro-1H-inden-1-one (475654-43-4)

Guidance literature:

With sodium hypochlorite; acetic acid; In water; at 0 - 17 ℃; for 3.33333h; regioselective reaction; Large scale;

DOI:10.1021/op700178q

Reference yield:

4-chloro-5-methoxy-2,3-dihydro-1H-inden-1-one (944109-65-3) + 4-(trifluoromethylthio)benzaldehyde (4021-50-5) → (E)-4-chloro-5-methoxy-2-(4-((trifluoromethyl)thio)benzylidene)-2,3-dihydro-1H-inden-1-one

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 120 ℃; for 6h;

upstream raw materials:

5-methoxy-1-indanone

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