tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate

Base Information

Chemical Name:tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate
CAS No.:1429187-72-3
Molecular Formula:C₁₇H₂₄Cl₂N₂O₄S
Molecular Weight:423.361
Hs Code.:

Synonyms:tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate

Suppliers and Price of tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate

There total 1 articles about tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-31-7
3,4-dichlorobenzenesulphonyl chloride

: 135632-53-0
tert-butyl N-(4-piperidinylmethyl)carbamate

: 1429187-72-3
tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methyl carbamate

Guidance literature:: With triethylamine; at 20 ℃; for 18h;

Reference yield: 98.0%

: 1429187-72-3
tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methyl carbamate

: 1154214-90-0
(1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methanamine

Guidance literature:: With hydrogenchloride; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1429187-72-3
tert-butyl (1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methyl carbamate

: 1429343-41-8
N-((1-(3,4-dichlorophenylsulfonyl)piperidin-4-yl)methyl)-4-hydroxy-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / dichloromethane / 16 h / 20 °C

2: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

3: boron tribromide-dimethyl sulfide complex / dichloromethane / 2 h / 70 °C

With 4-methyl-morpholine; hydrogenchloride; boron tribromide-dimethyl sulfide complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;