6-Tributylstannyl[1,2,4]triazolo[1,5-a]pyridine

Base Information

• Chemical Name: 6-Tributylstannyl[1,2,4]triazolo[1,5-a]pyridine
• CAS No.: 1159812-31-3
• Molecular Formula: C18H31N3Sn
• Molecular Weight: 212.049

Synonyms:6-Tributylstannyl[1,2,4]triazolo[1,5-a]pyridine;5-a]pyridine;6-Tributylstannyl[1;7-broMo-2-Methyl-[1;7-BroMo-2-Methyl-[1,2,4]triazolo[1,5-a]pyridine

Chemical Property of 6-Tributylstannyl[1,2,4]triazolo[1,5-a]pyridine

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Tributylstannyl[1,2,4]triazolo[1,5-a]pyridine

There total 3 articles about 6-Tributylstannyl[1,2,4]triazolo[1,5-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.8%

1,2-diamino-4-bromopyridin-1-ium-2,4,6-trimethylbenzenesulfonate (1202704-61-7) + acetic anhydride (108-24-7) → 7-bromo-2-methyl-[1,2,4]triazolo[1,5-a]pyridine (1159812-31-3)

Guidance literature:

With p-toluenesulfonic acid monohydrate; In ethanol; at 100 ℃; for 24h; Sealed tube;

Reference yield:

1,2-diamino-4-bromopyridin-1-ium 2,4,6-trimethylbenzenesulfonate + acetic anhydride (108-24-7) → 7-bromo-2-methyl-[1,2,4]triazolo[1,5-a]pyridine (1159812-31-3)

Guidance literature:

With toluene-4-sulfonic acid; at 100 ℃; Sealed tube;

Reference yield:

→ 7-bromo-2-methyl-[1,2,4]triazolo[1,5-a]pyridine (1159812-31-3)

Guidance literature:

upstream raw materials:

acetic anhydride

1,2-diamino-4-bromopyridin-1-ium-2,4,6-trimethylbenzenesulfonate

Downstream raw materials:

(S)-6-(2-hydroxy-2-methyl-propyl)-3-{(S)-1-[4-(2-methyl-[1,2,4]triazolo[1,5-a]pyridin-7-yl)-phenyl]-ethyl}-6-phenyl-[1,3]oxazinan-2-one

C₁₉H₁₆FN₇O₂

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