Potassium 3,3,3-trifluoropropane-1-trifluoroborate

Base Information

• Chemical Name: Potassium 3,3,3-trifluoropropane-1-trifluoroborate
• CAS No.: 1430722-07-8
• Molecular Formula: C3H4BF6K
• Molecular Weight: 203.964
• Hs Code.: 2931900090
• Mol file: 1430722-07-8.mol

Synonyms:Potassium 3,3,3-trifluoropropane-1-trifluoroborate;Potassium(3,3,3-trifluoroprop-1-yl)trifluoroborate

Chemical Property of Potassium 3,3,3-trifluoropropane-1-trifluoroborate

Chemical Property:

• PSA: 0.00000
• LogP: 2.78620

Purity/Quality:

99% ^*data from raw suppliers

Potassium3,3,3-trifluoropropane-1-trifluoroborate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Potassium 3,3,3-trifluoropropane-1-trifluoroborate

There total 2 articles about Potassium 3,3,3-trifluoropropane-1-trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium trifluoro(3,3,3-trifluoroprop-1-ynyl)boranuide (869583-61-9) → potassium (3,3,3-trifluoroprop-1-yl)trifluoroborate (1430722-07-8) + potassium [(E)-3,3,3-trifluoroprop-1-en-1-yl]trifluoroborate

Guidance literature:

With Lindlar catalyst; In methanol; at 20 ℃; for 1.5h; under 760.051 Torr; Solvent; Concentration; Reagent/catalyst; Time; stereoselective reaction; Inert atmosphere;

DOI:10.1021/acs.orglett.5b00235

Reference yield:

potassium trifluoro(3,3,3-trifluoroprop-1-ynyl)boranuide (869583-61-9) → potassium (3,3,3-trifluoroprop-1-yl)trifluoroborate (1430722-07-8) + potassium [(Z)-3,3,3-trifluoroprop-1-en-1-yl]trifluoroborate + potassium [(E)-3,3,3-trifluoroprop-1-en-1-yl]trifluoroborate

Guidance literature:

With Lindlar catalyst; In tetrahydrofuran; at 20 ℃; for 3.5h; under 760.051 Torr; Solvent; Concentration; Reagent/catalyst; Time; stereoselective reaction; Inert atmosphere;

DOI:10.1021/acs.orglett.5b00235

Reference yield: 96.0%

potassium (3,3,3-trifluoroprop-1-yl)trifluoroborate (1430722-07-8) + 6-bromo-2-(4-fluorophenyl)-5-isopropoxy-N-methylbenzofuran-3-carboxamide → 2-(4-fluorophenyl)-5-isopropoxy-N-methyl-6-(3,3,3-trifluoropropyl)benzofuran-3-carboxamide

Guidance literature:

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In water; toluene; at 90 ℃; for 16h; Inert atmosphere;

upstream raw materials:

potassium trifluoro(3,3,3-trifluoroprop-1-ynyl)boranuide

Downstream raw materials:

C₁₅H₁₄F₃N