XPhos Palladacycle Gen. 4

Base Information

• Chemical Name: XPhos Palladacycle Gen. 4
• CAS No.: 1599466-81-5
• Molecular Formula: C47H64NO3PPdS
• Molecular Weight: 860.49
• Mol file: 1599466-81-5.mol

Synonyms:(SP-4-3)-[Dicyclohexyl[2',4',6'-tris(1-methylethyl)[1,1'-biphenyl]-2-yl]phosphine](methanesulfonato)[2'-(methylamino)[1,1'-biphenyl]-2-yl]palladium;Methanesulfonato(2-dicyclohexylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-methylamino-1,1'-biphenyl-2-yl)palladium(II)

Chemical Property of XPhos Palladacycle Gen. 4

Chemical Property:

• PSA: 76.42000
• LogP: 13.84750

Purity/Quality:

99% ^*data from raw suppliers

Methanesulfonato(2-dicyclohexylphosphino-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-methylamino-1,1'-biphenyl-2-yl)palladium(II), min. 98% [XPhos Palladacycle Gen. 4] ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: A powerful ligand for classic cross-coupling reactions combined with the Buchwald Fourth Generation Palladacycle. Bench stable, soluble in most organic solvents.

Technology Process of XPhos Palladacycle Gen. 4

There total 1 articles about XPhos Palladacycle Gen. 4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(2′-methylamino-1,1′-biphenyl-2-yl)methanesulfonatopalladium(II) dimer (1581285-85-9) + XPhos (564483-18-7) → (2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II) methanesulfonate (1599466-81-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jo500355k

upstream raw materials:

(2′-methylamino-1,1′-biphenyl-2-yl)methanesulfonatopalladium(II) dimer

XPhos

Refernces