decahydro-1H-Cycloocta[c]pyrrole

Base Information

• Chemical Name: decahydro-1H-Cycloocta[c]pyrrole
• CAS No.: 119017-74-2
• Molecular Formula: C₁₀H₁₉N
• Molecular Weight: 153.268
• Mol file: 119017-74-2.mol

Synonyms:decahydro-1H-Cycloocta[c]pyrrole

Chemical Property of decahydro-1H-Cycloocta[c]pyrrole

Chemical Property:

• PSA: 12.03000
• LogP: 2.50500

Purity/Quality:

decahydro-1H-Cycloocta[c]pyrrole 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of decahydro-1H-Cycloocta[c]pyrrole

There total 5 articles about decahydro-1H-Cycloocta[c]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-benzyl-10-aza<6.3.0>bicycloundecane (118989-11-0) → 10-aza<6.3.0>bicycloundecane (119017-74-2)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol;

DOI:10.1016/S0040-4020(01)87128-3

Reference yield:

decahydro-cycloocta[c]pyrrol-1-one → 10-aza<6.3.0>bicycloundecane (119017-74-2)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; dichloromethane; at 20 ℃;

DOI:10.1021/ja011513o

Reference yield:

N-(1'-hydroxy-2'-butyl)-10-aza-6,3,0-bicycloundecane (118989-07-4) → 10-aza<6.3.0>bicycloundecane (119017-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaHCO₃; 2.) t-BuOK / 1.) MeOH; 2.) t-BuOH

2: HCOONH₄, 10percent Pd-C / methanol

With palladium on activated charcoal; potassium tert-butylate; ammonium formate; sodium hydrogencarbonate; In methanol;

DOI:10.1016/0040-4039(88)85195-5

upstream raw materials:

N-benzyl-10-aza<6.3.0>bicycloundecane

N-(1'-hydroxy-2'-butyl)-10-aza-6,3,0-bicycloundecane

N-(1'-t-butoxy-2'-butyl)-10-aza<6,3,0>bicycloundecane

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