6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine

Base Information

Chemical Name:6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine
CAS No.:110919-70-5
Molecular Formula:C₈H₉FN₂O
Molecular Weight:168.171
Hs Code.:
Mol file:110919-70-5.mol

Synonyms:6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine;N-(5-Fluoro-6-methylpyridin-2-yl)acetamide

Suppliers and Price of 6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine

There total 2 articles about 6-(Acetylamino)-3-fluoro-2-methylpyridine, 6-Acetamido-3-fluoro-2-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6-(acetylamino)-2-methyl-3-pyridinediazonium tetrafluoroborate

: 110919-70-5
N-(5-fluoro-6-methyl-2-pyridinyl)acetamide

Guidance literature:: In toluene; 1.) 100 deg C; 2.) reflux, 1 h.;
DOI:10.1002/jhet.5570240139

Reference yield:

: 5671-67-0
N-(5-amino-6-methyl-2-pyridinyl)acetamide

: 110919-70-5
N-(5-fluoro-6-methyl-2-pyridinyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂, 48percent HBF₄ / H₂O / 1 h / -10 °C

2: 80 percent / toluene / 1.) 100 deg C; 2.) reflux, 1 h.

With tetrafluoroboric acid; sodium nitrite; In water; toluene;
DOI:10.1002/jhet.5570240139