CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY)

Base Information

Chemical Name:CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY)
CAS No.:92456-55-8
Molecular Formula:C₁₀H₁₆N₄O₄
Molecular Weight:256.261
Hs Code.:
Mol file:92456-55-8.mol

Synonyms:CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY);CYCLO(B-ALA-GLY-BETA-ALA-GLY)

Suppliers and Price of CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY)

Chemical Property:

Boiling Point:857.8±65.0 °C (760 mmHg)
PSA：116.40000
Density:1.172±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:-1.43980
Storage Temp.:-15°C

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY)

There total 2 articles about CYCLO(-BETA-ALA-GLY-BETA-ALA-GLY) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1609650-99-8
Cbz-β-Ala-Gly-Bt

: 92456-55-8
cyclo(Gly-β-Ala-Gly-β-Ala)

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃;
DOI:10.1002/chem.201304262

Reference yield:

: 58171-88-3
Cbz-β-Ala-Gly-OH

: 92456-55-8
cyclo(Gly-β-Ala-Gly-β-Ala)

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / tetrahydrofuran / 0.33 h / -20 °C

1.2: 3 h / -20 - 20 °C

2.1: hydrogen; palladium 10% on activated carbon / methanol / 20 °C

With thionyl chloride; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201304262