Ethyl 6-oxaspiro[2.5]octane-1-carboxylate

Base Information

• Chemical Name: Ethyl 6-oxaspiro[2.5]octane-1-carboxylate
• CAS No.: 909406-74-2
• Molecular Formula: C₁₀H₁₆O₃
• Molecular Weight: 184.235
• Hs Code.: 2932990090
• Mol file: 909406-74-2.mol

Synonyms:Ethyl 6-oxaspiro[2.5]octane-1-carboxylate;6-Oxaspiro[2.5]octane-1-carboxylic acid ethyl ester

Chemical Property of Ethyl 6-oxaspiro[2.5]octane-1-carboxylate

Chemical Property:

• PSA: 35.53000
• LogP: 1.36620

Purity/Quality:

97% ^*data from raw suppliers

Ethyl6-oxaspiro[2.5]octane-1-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 6-oxaspiro[2.5]octane-1-carboxylate

There total 5 articles about Ethyl 6-oxaspiro[2.5]octane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl tetrahydro-4H-pyran-4-ylideneacetate (130312-00-4) → ethyl 6-oxaspiro[2.5]octane-1-carboxylate (909406-74-2)

Guidance literature:

trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 1.83333h;

ethyl tetrahydro-4H-pyran-4-ylideneacetate; In dimethyl sulfoxide; at 20 ℃; for 18h;

Reference yield:

ethyl tetrahydro-4H-pyran-4-ylideneacetate (130312-00-4) + trimethylsulphoxonium iodide (1030268-24-6) → ethyl 6-oxaspiro[2.5]octane-1-carboxylate (909406-74-2)

Guidance literature:

trimethylsulphoxonium iodide; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 2h;

ethyl tetrahydro-4H-pyran-4-ylideneacetate; In dimethyl sulfoxide; at 20 ℃; for 18h;

Reference yield:

ethyl tetrahydro-4H-pyran-4-ylideneacetate (130312-00-4) + trimethylsulfoxonium iodide (1774-47-6) → ethyl 6-oxaspiro[2.5]octane-1-carboxylate (909406-74-2)

Guidance literature:

trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; mineral oil; at 0 - 20 ℃; for 0.333333h;

ethyl tetrahydro-4H-pyran-4-ylideneacetate; In dimethyl sulfoxide; mineral oil; at 20 ℃; for 18h;

upstream raw materials:

ethyl tetrahydro-4H-pyran-4-ylideneacetate

trimethylsulphoxonium iodide

trimethylsulfoxonium iodide

Tetrahydro-4H-pyran-4-one

Downstream raw materials:

6-oxaspiro[2.5]octane-1-carboxylic acid

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