1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid

Base Information

• Chemical Name: 1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid
• CAS No.: 521985-24-0
• Molecular Formula: C8H9BN2O2
• Molecular Weight: 175.983
• Hs Code.: 2933998090
• Mol file: 521985-24-0.mol

Synonyms:1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid;Boronic acid, (1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl)- (9CI);(1-methyl-1H-pyrrolo[2,3-b]pyridin-3-yl)Boronic acid

Chemical Property of 1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid

Chemical Property:

• PSA: 58.28000
• LogP: -0.74690

Purity/Quality:

97% ^*data from raw suppliers

1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid ^*data from reagent suppliers

Safty Information:

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Technology Process of 1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid

There total 1 articles about 1-Methyl-1H-pyrrolo[2,3-b]pyridin-3-yl-3-boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-1H-pyrrolo[2,3-b]pyridine (27257-15-4) → 1-methyl-1H-pyrrolo[2,3-b]pyridine-3-boric acid (521985-24-0)

Guidance literature:

1-methyl-1H-pyrrolo[2,3-b]pyridine; With tert.-butyl lithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

With Triisopropyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h;

With water; In tetrahydrofuran; hexane; at 20 ℃; for 0.666667h;

Reference yield:

1-methyl-1H-pyrrolo[2,3-b]pyridine-3-boric acid (521985-24-0) + 1-Bromo-4-fluorobenzene (460-00-4) → 2-(4-fluorophenyl)-1-methyl-1H-pyrrolo[2,3-b]pyridine (521985-25-1)

Guidance literature:

With sodium hydrogencarbonate; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 80 ℃; for 17h;

upstream raw materials:

1-methyl-1H-pyrrolo[2,3-b]pyridine

Downstream raw materials:

2-(4-fluorophenyl)-1-methyl-1H-pyrrolo[2,3-b]pyridine

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