Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI)

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI)
CAS No.:40929-75-7
Molecular Formula:C9H13NO2
Molecular Weight:167.20502
Hs Code.:2926909090
Mol file:40929-75-7.mol

Synonyms:Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI)

Suppliers and Price of Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI)

Chemical Property:

PSA：26.30000
LogP:1.01230

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI)

There total 5 articles about Cyclohexanecarboxylic acid, 1-isocyano-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.5%

: 51642-05-8
N-Formyl-1-aminocyclohexanecarboxylic acid methyl ester

: 40929-75-7
methyl 1-isocyanocyclohexane-1-carboxylate

Guidance literature:: With bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; 1.) -10 deg C, 5 min, 2.) r.t., 4 h;
DOI:10.1055/s-1998-2103

Reference yield: 45.0%

: 17640-15-2
methyl cyanoformate

: (1-isocyanocyclohexyl)(2-methoxyphenyl)sulfane

: 40929-75-7
methyl 1-isocyanocyclohexane-1-carboxylate

Guidance literature:: (1-isocyanocyclohexyl)(2-methoxyphenyl)sulfane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

methyl cyanoformate; In tetrahydrofuran; at -78 - 20 ℃; for 2h;
DOI:10.1021/acs.orglett.8b02574

Reference yield: 44.0%

: 109-72-8,29786-93-4
n-butyllithium

: 17640-15-2
methyl cyanoformate

: (1-isocyanocyclohexyl)(2-methoxyphenyl)sulfane

: 40929-75-7
methyl 1-isocyanocyclohexane-1-carboxylate

: 100789-96-6
n-butyl 2-methoxyphenyl sulfide

Guidance literature:: n-butyllithium; (1-isocyanocyclohexyl)(2-methoxyphenyl)sulfane; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

methyl cyanoformate; In tetrahydrofuran; at -78 - 20 ℃; for 3h; Solvent; Temperature; Inert atmosphere;