3-METHOXY-2-PROPOXYBENZALDEHYDE OXIME

Base Information

• Chemical Name: 3-METHOXY-2-PROPOXYBENZALDEHYDE OXIME
• CAS No.: 41828-04-0
• Molecular Formula: C₁₁H₁₅NO₃
• Molecular Weight: 209.245
• Hs Code.: 2928000090
• Mol file: 41828-04-0.mol

Synonyms:3-METHOXY-2-PROPOXYBENZALDEHYDE OXIME

Chemical Property of 3-METHOXY-2-PROPOXYBENZALDEHYDE OXIME

Chemical Property:

• PSA: 51.05000
• LogP: 2.29210

Purity/Quality:

98%min ^*data from raw suppliers

3-methoxy-2-propoxybenzaldehydeoxime ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-METHOXY-2-PROPOXYBENZALDEHYDE OXIME

There total 2 articles about 3-METHOXY-2-PROPOXYBENZALDEHYDE OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-2-propoxy-benzaldehyde (41828-10-8) → 2-n-Propoxy-3-methoxy-benzaldoxim (41828-04-0)

Guidance literature:

With hydroxylamine hydrochloride; sodium carbonate;

Reference yield:

→ 2-n-Propoxy-3-methoxy-benzaldoxim (41828-04-0)

Guidance literature:

entspr. Benzaldehyd, H2NOH-HCl;

Reference yield: 65.0%

2-n-Propoxy-3-methoxy-benzaldoxim (41828-04-0) → 3-methoxy-2-propoxyphenylmethanamine hydrochloride (89411-11-0)

Guidance literature:

2-n-Propoxy-3-methoxy-benzaldoxim; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 4h; Reflux;

With hydrogenchloride; In 1,4-dioxane; ethyl acetate;

DOI:10.1134/S1070428010070110

upstream raw materials:

3-methoxy-2-propoxy-benzaldehyde

Downstream raw materials:

2-n-Propoxy-3-methoxy-benzonitril

3-methoxy-2-propoxyphenylmethanamine hydrochloride

Refernces

• 1、 PROFFT,SCHINDLER. "On the knowledge of o-vanillin. Part VI. Keto bases of pyrocatechol.". . p. 375 - 383. Retrieved 2007/10/05.