tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate

Base Information

Chemical Name:tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate
CAS No.:1378608-46-8
Molecular Formula:C10H18N2O2
Molecular Weight:198.26212
Hs Code.:
Mol file:1378608-46-8.mol

Synonyms:tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate

Suppliers and Price of tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(1-cyano-2-methylpropan-2-yl)carbamate 95+%
1g
$ 455.00

Total 9 raw suppliers

Chemical Property of tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(1-cyano-2-methylpropan-2-yl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate

There total 5 articles about tert-butyl 1-cyano-2-Methylpropan-2-ylcarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 113486-06-9
(1,1-dimethyl-prop-2-ynyl)-carbamic acid tert-butyl ester

: 1378608-46-8
tert-butyl (1-cyano-2-methylpropan-2-yl)carbamate

Guidance literature:: With trifuran-2-yl-phosphane; (hydridotris(1-pyrazolyl)borato)bis(ethylene)rhodium(I); tert-butylhydrazine; In 1,4-dioxane; at 100 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.6b00116

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 3-azido-3-methylbutanenitrile

: 1378608-46-8
tert-butyl (1-cyano-2-methylpropan-2-yl)carbamate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; under 3102.97 Torr;
DOI:10.1021/acs.jmedchem.6b01163

Reference yield:

: C₅H₁₀N₄O

: 1378608-46-8
tert-butyl (1-cyano-2-methylpropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 3102.97 Torr

With palladium 10% on activated carbon; hydrogen; acetic anhydride; In methanol;
DOI:10.1021/acs.jmedchem.6b01163