2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate)

Base Information

Chemical Name:2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate)
CAS No.:184698-69-9
Molecular Formula:C36H34Cl3NO7
Molecular Weight:699.027
Hs Code.:
Mol file:184698-69-9.mol

Synonyms:2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate)

Suppliers and Price of 2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate)

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate)

There total 1 articles about 2,3,4-Tris-O-(phenylmethyl)-alpha-D-glucopyranuronic acid phenylmethyl ester 1-(2,2,2-trichloroethanimidate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4539-78-0
2,3,4-tri-O-benzyl-D-glucopyranosideuronic acid benzyl ester

: 545-06-2
trichloroacetonitrile

: 184698-69-9,159420-94-7
benzyl 2,3,4-tri-O-benzyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

Guidance literature:: DOI:10.1016/S0040-4039(00)01556-2

Reference yield: 74.0%

: 454-92-2
3-(trifluoromethyl)benzoic acid

: 184698-69-9,159420-94-7
benzyl 2,3,4-tri-O-benzyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: benzyl 2,3,4-tri-O-benzyl-1-O-(3-(trifluoromethyl)benzoyl)-β-D-glucopyranuronoate

Guidance literature:: With molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at -20 - 20 ℃; for 4h;
DOI:10.1021/tx960047r

Reference yield: 50.0%

: 1607445-07-7
ethyl 6-O-acetyl-4-O-benzyl-3-O-(2-naphthalenylmethyl)-1-thio-α-D-mannopyranoside

: 184698-69-9,159420-94-7
benzyl 2,3,4-tri-O-benzyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate

: ethyl [benzyl (2,3,4-tri-O-benzyl-β-D-glucopyranosyl)uronate]-(1→2)-6-O-acetyl-4-O-benzyl-3-O-(2-methylnaphthalenyl)-1-thio-α-D-mannopyranoside

: ethyl [benzyl (2,3,4-tri-O-benzyl-α-D-glucopyranosyl)uronate]-(1→2)-6-O-acetyl-4-O-benzyl-3-O-(2-methylnaphthalenyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 1h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2014.01.022