Furan, 5-ethoxytetrahydro-2-methyl-3-(phenylmethylene)-, (3Z)- (9CI)

Base Information

• Chemical Name: Furan, 5-ethoxytetrahydro-2-methyl-3-(phenylmethylene)-, (3Z)- (9CI)
• CAS No.: 333754-63-5
• Molecular Formula: C₁₄H₁₈O₂
• Molecular Weight: 218.296
• Mol file: 333754-63-5.mol

Synonyms:Furan, 5-ethoxytetrahydro-2-methyl-3-(phenylmethylene)-, (3Z)- (9CI)

Chemical Property of Furan, 5-ethoxytetrahydro-2-methyl-3-(phenylmethylene)-, (3Z)- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Furan, 5-ethoxytetrahydro-2-methyl-3-(phenylmethylene)-, (3Z)- (9CI)

There total 2 articles about Furan, 5-ethoxytetrahydro-2-methyl-3-(phenylmethylene)-, (3Z)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[3-(1-ethoxy-2-iodo-ethoxy)-but-1-ynyl]-benzene → 5-Ethoxy-2-methyl-3-[1-phenyl-meth-(Z)-ylidene]-tetrahydro-furan (333754-63-5) + 5-Ethoxy-2-methyl-3-[1-phenyl-meth-(E)-ylidene]-tetrahydro-furan (333754-63-5)

Guidance literature:

With triethyl borane; tris(2,6-diphenylbenzyl)tin hydride; In hexane; dichloromethane; at -78 ℃; Further Variations:; Reagents; Product distribution;

DOI:10.1002/1521-3773(20010119)40:2<411::AID-ANIE411>3.0.CO;2-I

Reference yield:

[3-(1-ethoxy-2-iodo-ethoxy)-but-1-ynyl]-benzene → 5-Ethoxy-2-methyl-3-[1-phenyl-meth-(Z)-ylidene]-tetrahydro-furan (333754-63-5) + 5-Ethoxy-2-methyl-3-[1-phenyl-meth-(E)-ylidene]-tetrahydro-furan (333754-63-5)

Guidance literature:

With triethyl borane; tris(2,6-diphenylbenzyl)tin hydride; In hexane; dichloromethane; at -78 ℃; Further Variations:; Reagents; Product distribution;

DOI:10.1002/1521-3773(20010119)40:2<411::AID-ANIE411>3.0.CO;2-I