(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE

Base Information

Chemical Name:(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE
CAS No.:568543-67-9
Molecular Formula:C12H11N3OS
Molecular Weight:245.3
Hs Code.:
Mol file:568543-67-9.mol

Synonyms:(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE;1,4,5,6,7,8-hexahydro-4-oxo-[1]Benzothieno[2,3-d]pyrimidin-2-acetonitrile

Suppliers and Price of (4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE 95.00%
5G
$ 1548.26

American Custom Chemicals Corporation
(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE 95.00%
2.5G
$ 1227.82

American Custom Chemicals Corporation
(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE 95.00%
1G
$ 852.55

Total 3 raw suppliers

Chemical Property of (4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE

Chemical Property:

Melting Point:139 °C (dimethylformamide)
PSA：97.78000
LogP:1.92948

Purity/Quality:

97% ^*data from raw suppliers

(4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE

There total 1 articles about (4-OXO-3,4,5,6,7,8-HEXAHYDRO-BENZO[4,5]THIENO[2,3-D]PYRIMIDIN-2-YL)-ACETONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 109-77-3
malononitrile

: 4815-28-5
2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxamide

: 568543-67-9
4-hydroxy-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-d]pyrimidine-2-acetonitrile

Guidance literature:: With triethylamine; In ethanol; for 6h; Heating;
DOI:10.1002/hc.10179

Reference yield: 95.0%

: 568543-67-9
C₁₂H₁₁N₃OS

: 17422-74-1
3-Formylchromone

: 872103-08-7
9-(2-hydroxybenzoyl)-12-oxo-1,2,3,4-tetrahydro-12H-[1]benzothieno[2,3-d]pyrido[1,2-a]pyrimidine-7-carbonitrile

Guidance literature:: With chloro-trimethyl-silane; In N,N-dimethyl-formamide; for 12h; Heating;
DOI:10.1055/s-2008-1066988

Reference yield: 80.0%

: 62-53-3
aniline

: 568543-67-9
4-hydroxy-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-d]pyrimidine-2-acetonitrile

: 4-hydroxy-α-(phenylhydrazono)-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-d]pyrimidine-2-acetonitrile

Guidance literature:: aniline; With hydrogenchloride; sodium nitrite;

4-hydroxy-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-d]pyrimidine-2-acetonitrile; With sodium acetate; In ethanol; at 20 ℃; for 0.5h;
DOI:10.1002/hc.10179