4-FLUORO-3-METHYLPHENYLACETIC ACID

Base Information

• Chemical Name: 4-FLUORO-3-METHYLPHENYLACETIC ACID
• CAS No.: 1000520-92-2
• Molecular Formula: C₉H₉FO₂
• Molecular Weight: 168.168
• Mol file: 1000520-92-2.mol

Synonyms:4-fluoro-3-methylphenylacetic aicd;RARECHEM AL MS 0051;OTAVA-BB 1312887;2-(4-Fluoro-3-methylphenyl)acetic acid

Chemical Property of 4-FLUORO-3-METHYLPHENYLACETIC ACID

Chemical Property:

• PSA: 37.30000
• LogP: 1.76120

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-FLUORO-3-METHYLPHENYLACETIC ACID

There total 1 articles about 4-FLUORO-3-METHYLPHENYLACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

→ (4-fluoro-3-methylphenyl)acetic acid (1000520-92-2)

Guidance literature:

With potassium phosphate; tri-1-napthylphosphine; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; at 20 ℃; Sealed tube; Inert atmosphere;

With lithium hydroxide; In tetrahydrofuran; at 20 ℃;

Reference yield:

(2-(2-aminopyridin-4-yl)-5-methyl-3-(phenylamino)-1,5,6,7-tetrahydro-4H-pyrrolo[3,2-c]pyridin-4-one) + (4-fluoro-3-methylphenyl)acetic acid (1000520-92-2) → N-[4-(3-anilino-5-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-2-yl)pyridin-2-yl]-2-(4-fluoro-3-methylphenyl)acetamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 60 ℃; for 16h;

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