H6BTE

Base Information

• Chemical Name: H6BTE
• CAS No.: 1173285-13-6
• Molecular Formula: C36H18O12
• Molecular Weight: 642.532
• Mol file: 1173285-13-6.mol

Synonyms:H6BTE;1,3,5-Tris(3,5-dicarboxyphenylethynyl)benzene

Chemical Property of H6BTE

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of H6BTE

There total 2 articles about H6BTE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.9%

C42H30O12 (1192621-78-5) → 5,5',5''-benzene-1,3,5-triyltris(1-ethynyl-2-isophthalic acid) (1173285-13-6)

Guidance literature:

C₄₂H₃₀O₁₂; With sodium hydroxide; In methanol; at 80 ℃; for 5h;

With hydrogenchloride; water; for 5h; pH=2 - 3;

DOI:10.1039/b909250a

Reference yield:

1,3,5-tris(2-diethyl isophthalate-1-ethynyl)benzene (1173285-11-4) → 5,5',5''-benzene-1,3,5-triyltris(1-ethynyl-2-isophthalic acid) (1173285-13-6)

Guidance literature:

With water; potassium hydroxide; In tetrahydrofuran; for 4h; Reflux;

DOI:10.1021/ja901109t

Reference yield:

copper(II) nitrate trihydrate + 5,5',5''-benzene-1,3,5-triyltris(1-ethynyl-2-isophthalic acid) (1173285-13-6) → Cu24(1,3,5-tris(3,5-dicarboxylphenylethynyl)benzene)8(H2O)12

Guidance literature:

With HCl; In N,N-dimethyl-formamide; High Pressure; solvothermal reaction of Cu(NO3)2*6H2O with acid in DMF in presence of small amount of HCl;

DOI:10.1039/b909250a

upstream raw materials:

1,3,5-tris(2-diethyl isophthalate-1-ethynyl)benzene

C₄₂H₃₀O₁₂