1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution)

Base Information

Chemical Name:1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution)
CAS No.:128723-16-0
Molecular Formula:C₂₇H₄₄O₃
Molecular Weight:0
Hs Code.:

Synonyms:1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution);1α,25-Dihydroxyvitamin D3 (6,19,19-d3) ;1α,25-Dihydroxycholecalciferol (6,19,19-d3) solution;Calcitriol (6,19,19-d3) solution;Deuterated 1-α25-Dihydroxyvitamin D3 solution

Suppliers and Price of 1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution)

Chemical Property:

Flash Point:14 °C

Purity/Quality:: 96% by CP; 97% atom D ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution)

There total 8 articles about 1,25-Dihydroxyvitamin D3-[D3] (CertiMass solution) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 140710-99-2,140711-00-8,140711-01-9
1α,25-dihydroxy-5Z-<6,19,19'-2H3>vitamin D3-3β-tert-butyldimethylsilyl ether

: 128723-16-0
1α,25-dihydroxy-5Z-<6,19,19'-2H3>vitamin D3

Guidance literature:: With hydrogen fluoride; In acetonitrile; at 25 ℃; for 1.5h;
DOI:10.1016/0039-128X(92)90072-H

Reference yield:

: 140710-95-8
(4S,6R)-1-[(1R,3aS,7aR)-1-((R)-5-Hydroxy-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidenemethyl]-2,2-dioxo-2,3,4,5,6,7-hexahydro-1H-2λ⁶-benzo[c]thiophene-4,6-diol

: 128723-16-0
C₂₇H₄₁⁽²⁾H₃O₃

Guidance literature:: With potassium tert-butylate; water-d2; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h;
DOI:10.1016/0039-128X(92)90072-H

Reference yield:

: 32222-06-3
calcitriol

: 128723-16-0
C₂₇H₄₁⁽²⁾H₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: SO₂ (l) / 1 h / Heating

2: t-BuOK, D₂O / dimethylformamide / 0.5 h / 25 °C

3: ethanol; toluene / 1 h / 60 °C

With sulfur dioxide; potassium tert-butylate; water-d2; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0039-128X(92)90072-H