3-Chloro-3-methylbutylbenzene

Base Information

• Chemical Name: 3-Chloro-3-methylbutylbenzene
• CAS No.: 4830-95-9
• Molecular Formula: C11H15Cl
• Molecular Weight: 182.693
• Mol file: 4830-95-9.mol

Synonyms:(3-Chloro-3-methylbutyl)benzene;1-Phenyl-3-chloro-3-methylbutane;3-Chloro-3-methylbutylbenzene

Chemical Property of 3-Chloro-3-methylbutylbenzene

Chemical Property:

• Boiling Point: 125-126 °C(Press: 15 Torr)
• PSA: 0.00000
• Density: 0.997±0.06 g/cm3(Predicted)
• LogP: 3.92860

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Chloro-3-methylbutylbenzene

There total 11 articles about 3-Chloro-3-methylbutylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-phenyl-2-methyl-2-butanol (103-05-9) → 2-chloro-2-methyl-4-phenylbutane (4830-95-9)

Guidance literature:

With chloro-trimethyl-silane; In neat (no solvent); at 70 - 75 ℃; for 24h; chemoselective reaction; Green chemistry;

DOI:10.1016/j.tetlet.2016.04.083

Reference yield: 86.0%

4-phenyl-2-methyl-2-butanol (103-05-9) → 3-methyl-1-phenylbut-2-ene (4489-84-3) + 2-chloro-2-methyl-4-phenylbutane (4830-95-9)

Guidance literature:

With 1-pyrrolidinecarboxaldehyde; phenyl chloroformate; In tetrahydrofuran; at 80 ℃; chemoselective reaction;

DOI:10.1002/cctc.202001175

Reference yield: 84.0%

2-methyl-4-phenyl-1-butene (6683-51-8) → 2-chloro-2-methyl-4-phenylbutane (4830-95-9)

Guidance literature:

With methanesulfonic acid; acetic acid; calcium chloride; at 20 ℃; for 5h;

DOI:10.1055/s-0040-1719856

upstream raw materials:

4-phenyl-2-methyl-2-butanol

3-methoxy-3-methyl-1-phenylbutane

1-methoxy-2-methyl-1-trimethylsiloxy-1-propene

2-fluoro-2-methyl-4-phenylbutane

Downstream raw materials:

3-methyl-1-phenylbut-2-ene

(3-methylbutyl)benzene

1,1-dimethylindan

1-(1,1-dimethyl-3-phenylpropyl)-1H-indene