4-(N-(1-NAPHTHYL)-N-PHENYLAMINO)-4'-BROMOBIPHENYL

Base Information

• Chemical Name: 4-(N-(1-NAPHTHYL)-N-PHENYLAMINO)-4'-BROMOBIPHENYL
• CAS No.: 352359-42-3
• Molecular Formula: C28H20BrN
• Molecular Weight: 450.377
• Mol file: 352359-42-3.mol

Synonyms:N-(4'-bromo-[1,1'-biphenyl]-4-yl)-N-phenylnaphthalen-1-amine;N-(4-bromo[1,1-biphenyl]-4-yl)-N-phenyl-1-Naphthalenamine;N-(4'-bromobiphenyl-4-yl)-N-phenylnaphthalen-1-amine;N-(4'-Bromo-4-biphenylyl)-N-phenyl-1-naphthylamine;N-(4'-Bromo-4-biphenylyl)-N-phenyl-1-naphthylamine

Chemical Property of 4-(N-(1-NAPHTHYL)-N-PHENYLAMINO)-4'-BROMOBIPHENYL

Chemical Property:

• Melting Point: 167.0 to 171.0 °C
• PSA: 3.24000
• LogP: 8.73910

Purity/Quality:

97% ^*data from raw suppliers

N-(4'-Bromo-4-biphenylyl)-N-phenyl-1-naphthylamine >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(N-(1-NAPHTHYL)-N-PHENYLAMINO)-4'-BROMOBIPHENYL

There total 7 articles about 4-(N-(1-NAPHTHYL)-N-PHENYLAMINO)-4'-BROMOBIPHENYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4-(4-bromophenyl)bromobenzene (92-86-4) + N-phenyl-1-naphthylamine (90-30-2) → N-(4’-bromo-[1,1‘-biphenyl]-4-yl)-N-phenylnaphthalen-1-amine (352359-42-3)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In toluene; at 100 ℃; for 7h;

DOI:10.1021/ma048365h

Reference yield: 66.0%

N-phenyl-1-naphthylamine (90-30-2) + 4-bromo-4'-iodobiphenyl (105946-82-5) → N-(4’-bromo-[1,1‘-biphenyl]-4-yl)-N-phenylnaphthalen-1-amine (352359-42-3)

Guidance literature:

With copper; potassium carbonate; sodium sulfate; In nitrobenzene;

Reference yield: 66.0%

→ N-(4’-bromo-[1,1‘-biphenyl]-4-yl)-N-phenylnaphthalen-1-amine (352359-42-3)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In dichloromethane; toluene; at 70 ℃;

upstream raw materials:

4-(4-bromophenyl)bromobenzene

N-phenyl-1-naphthylamine

N-Phenyl-2-naphthylamine

4-bromo-4'-iodobiphenyl

Downstream raw materials:

N-(1-Naphthyl)-N,N'-diphenylbenzidine

2-(N-1-naphthyl-N-phenylamino)-7-(N-phenylamino)phenanthrene

4’-[1-naphthyl(phenyl)amino]biphenyl-4-ylboronic acid

C₄₁H₃₁N₃

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